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@PHDTHESIS{Betz:10054,
author = {Betz, Michael},
title = {{H}erstellung und {C}harakterisierung von
sauerstoffionenleitenden {D}ünnschichtmembranstrukturen},
volume = {61},
issn = {1866-1793},
type = {Dr. (Univ.)},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {PreJuSER-10054},
isbn = {978-3-89336-618-7},
series = {Schriften des Forschungszentrums Jülich : Energie $\&$
Umwelt / Energy $\&$ Environment},
pages = {61 S.},
year = {2010},
note = {Record converted from VDB: 12.11.2012; Ruhr-Universität
Bochum},
abstract = {In power plants using Oxyfuel technology, fossil fuels are
combusted with pure oxygen. This leads to carbon dioxide of
high purity, which is necessary for its transport and
storage. Oxygen separation by means of perovskitic membranes
have great potential to decrease the efficiency losses
caused by the allocation of the enormous amounts of oxygen.
The aim of this work is the preparation and characterisation
of thin film membranes on porous substrates and the analysis
of their oxygen permeation properties. Therefore the
material system
A$_{0,68}$Sr$_{0,3}$Fe$_{0,8}$Co$_{0,2}$O$_{3−\delta}$
(A68SFC) was analysed, where the A-site was substituted with
Lanthanides (La, Pr, Nd, Eu, Sm, Gd, Dy, Er) or alkaline
earth metals (Ba, Ca). After an extensive characterisation,
the selection was reduced to the substitutions with La, Pr
and Nd. Other compounds could not meet the demands with
regard to phase purity, chemical stability or extension
behaviour. All analyses were conducted in comparison to
Ba$_{0,5}$Sr$_{0,5}$Co$_{0,8}$Fe$_{0,2}$O$_{3−\delta}$
(BSCF) which is known to exhibit higher permeation rates,
but is more sensitive to stability issues. The dependency of
permeation rates on membrane thickness or oxygen partial
pressures on both membrane surfaces is discussed by means of
permeation measurements conducted on bulk BSCF membranes.
These cannot be described completely by the Wagner equation.
This is due to changes of the driving force originating from
influences of the surface reaction kinetics and
concentration polarisation on the membrane surface, which
are not considered. Porous substrates for asymmetric
membranes were manufactured by tape casting and warm
pressing. The application of the functional layer was
performed via screen printing. Permeation measurements show
that the asymmetric structures exhibit higher permeation
rates in comparison to bulk membranes with L=1 mm. The
moderate increase can be attributed to the low gas
permeability of the substrates used.},
cin = {IEF-1},
ddc = {333.7},
cid = {I:(DE-Juel1)VDB809},
pnm = {Rationelle Energieumwandlung},
pid = {G:(DE-Juel1)FUEK402},
typ = {PUB:(DE-HGF)11 / PUB:(DE-HGF)3},
url = {https://juser.fz-juelich.de/record/10054},
}