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001005781 1001_ $$0P:(DE-HGF)0$$aBasak, Shibarata$$b0$$eCorresponding author
001005781 245__ $$aScreening of Coatings for an All-Solid-State Battery using In Situ Transmission Electron Microscopy
001005781 260__ $$aCambridge, MA$$bJoVE$$c2023
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001005781 520__ $$aWith the ever-increasing use of Li-ion batteries, especially due to their adoption in electric vehicles, their safety is in prime focus. Thus, the all-solid-state batteries (ASSBs) that use solid electrolytes instead of liquid electrolytes, which reduce the risk of flammability, have been the center stage of battery research for the last few years. However, in the ASSB, the ion transportation through the solid-solid electrolyte-electrode interface poses a challenge due to contact and chemical/electrochemical stability issues. Applying a suitable coating around the electrode and/or electrolyte particles offers a convenient solution, leading to better performance. For this, researchers are screening potential electronic/ionic conductive and nonconductive coatings to find the best coatings with suitable thickness for long-term chemical, electrochemical, and mechanical stability. Operando transmission electron microscopy (TEM) couples high spatial resolution with high temporal resolution to allow visualization of dynamic processes, and thus is an ideal tool to evaluate electrode/electrolyte coatings via studying (de)lithiation at a single particle level in real-time. However, the accumulated electron dose during a typical high-resolution in situ work may affect the electrochemical pathways, evaluation of which can be time-consuming. The current protocol presents an alternative procedure in which the potential coatings are applied on Si nanoparticles and are subjected to (de)lithiation during operando TEM experiments. The high volume changes of Si nanoparticles during (de)lithiation allow monitoring of the coating behavior at a relatively low magnification. Thus, the whole process is very electron-dose efficient and offers quick screening of potential coatings.
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001005781 536__ $$0G:(DE-HGF)POF4-5353$$a5353 - Understanding the Structural and Functional Behavior of Solid State Systems (POF4-535)$$cPOF4-535$$fPOF IV$$x1
001005781 536__ $$0G:(DE-HGF)POF4-1223$$a1223 - Batteries in Application (POF4-122)$$cPOF4-122$$fPOF IV$$x2
001005781 536__ $$0G:(EU-Grant)892916$$aElectroscopy - Electrochemistry of All-solid-state-battery Processes using Operando Electron Microscopy (892916)$$c892916$$fH2020-MSCA-IF-2019$$x3
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001005781 7001_ $$0P:(DE-Juel1)180853$$aPark, Junbeom$$b1
001005781 7001_ $$0P:(DE-Juel1)180678$$aJo, Janghyun$$b2
001005781 7001_ $$0P:(DE-Juel1)180631$$aCamara, Osmane$$b3
001005781 7001_ $$0P:(DE-Juel1)157886$$aTavabi, Amir H.$$b4
001005781 7001_ $$0P:(DE-Juel1)161208$$aTempel, Hermann$$b5
001005781 7001_ $$0P:(DE-Juel1)157700$$aKungl, Hans$$b6
001005781 7001_ $$0P:(DE-HGF)0$$aGeorge, Chandramohan$$b7
001005781 7001_ $$0P:(DE-Juel1)144121$$aDunin-Borkowski, Rafal E.$$b8
001005781 7001_ $$0P:(DE-Juel1)130824$$aMayer, Joachim$$b9
001005781 7001_ $$0P:(DE-Juel1)156123$$aEichel, Rüdiger-A.$$b10
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001005781 8564_ $$uhttps://juser.fz-juelich.de/record/1005781/files/Invoice_2022-707.pdf
001005781 8564_ $$uhttps://juser.fz-juelich.de/record/1005781/files/Screening%20of%20coatings.pdf$$yPublished on 2023-01-20. Available in OpenAccess from 2025-01-20.
001005781 8564_ $$uhttps://juser.fz-juelich.de/record/1005781/files/jove-protocol-64316-screening-coatings-for-an-all-solid-state-battery-using-situ.pdf$$yPublished on 2023-01-20. Available in OpenAccess from 2025-01-20.
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