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@ARTICLE{Basak:1005781,
      author       = {Basak, Shibarata and Park, Junbeom and Jo, Janghyun and
                      Camara, Osmane and Tavabi, Amir H. and Tempel, Hermann and
                      Kungl, Hans and George, Chandramohan and Dunin-Borkowski,
                      Rafal E. and Mayer, Joachim and Eichel, Rüdiger-A.},
      title        = {{S}creening of {C}oatings for an {A}ll-{S}olid-{S}tate
                      {B}attery using {I}n {S}itu {T}ransmission {E}lectron
                      {M}icroscopy},
      journal      = {JoVE science education},
      volume       = {191},
      issn         = {1940-087X},
      address      = {Cambridge, MA},
      publisher    = {JoVE},
      reportid     = {FZJ-2023-01626},
      pages        = {64316},
      year         = {2023},
      abstract     = {With the ever-increasing use of Li-ion batteries,
                      especially due to their adoption in electric vehicles, their
                      safety is in prime focus. Thus, the all-solid-state
                      batteries (ASSBs) that use solid electrolytes instead of
                      liquid electrolytes, which reduce the risk of flammability,
                      have been the center stage of battery research for the last
                      few years. However, in the ASSB, the ion transportation
                      through the solid-solid electrolyte-electrode interface
                      poses a challenge due to contact and
                      chemical/electrochemical stability issues. Applying a
                      suitable coating around the electrode and/or electrolyte
                      particles offers a convenient solution, leading to better
                      performance. For this, researchers are screening potential
                      electronic/ionic conductive and nonconductive coatings to
                      find the best coatings with suitable thickness for long-term
                      chemical, electrochemical, and mechanical stability.
                      Operando transmission electron microscopy (TEM) couples high
                      spatial resolution with high temporal resolution to allow
                      visualization of dynamic processes, and thus is an ideal
                      tool to evaluate electrode/electrolyte coatings via studying
                      (de)lithiation at a single particle level in real-time.
                      However, the accumulated electron dose during a typical
                      high-resolution in situ work may affect the electrochemical
                      pathways, evaluation of which can be time-consuming. The
                      current protocol presents an alternative procedure in which
                      the potential coatings are applied on Si nanoparticles and
                      are subjected to (de)lithiation during operando TEM
                      experiments. The high volume changes of Si nanoparticles
                      during (de)lithiation allow monitoring of the coating
                      behavior at a relatively low magnification. Thus, the whole
                      process is very electron-dose efficient and offers quick
                      screening of potential coatings.},
      cin          = {ER-C-1 / ER-C-2 / IEK-9},
      ddc          = {570},
      cid          = {I:(DE-Juel1)ER-C-1-20170209 / I:(DE-Juel1)ER-C-2-20170209 /
                      I:(DE-Juel1)IEK-9-20110218},
      pnm          = {5351 - Platform for Correlative, In Situ and Operando
                      Characterization (POF4-535) / 5353 - Understanding the
                      Structural and Functional Behavior of Solid State Systems
                      (POF4-535) / 1223 - Batteries in Application (POF4-122) /
                      Electroscopy - Electrochemistry of All-solid-state-battery
                      Processes using Operando Electron Microscopy (892916)},
      pid          = {G:(DE-HGF)POF4-5351 / G:(DE-HGF)POF4-5353 /
                      G:(DE-HGF)POF4-1223 / G:(EU-Grant)892916},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {36744797},
      UT           = {WOS:000992758700008},
      doi          = {10.3791/64316},
      url          = {https://juser.fz-juelich.de/record/1005781},
}