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@ARTICLE{Camara:1006877,
      author       = {Camara, Osmane and Xu, Qi and Park, Junbeom and Yu,
                      Shicheng and Lu, Xin and Dzieciol, Krzysztof and Schierholz,
                      Roland and Tempel, Hermann and Kungl, Hans and Chandramohan,
                      George and Mayer, Joachim and Basak, Shibabrata and Eichel,
                      Rüdiger-A.},
      title        = {{E}ffect of {L}ow {E}nvironmental {P}ressure on {S}intering
                      {B}ehavior of{NASICON}-{T}ype {L}i1.3{A}l0.3{T}i1.7({PO}4)3
                      {S}olid {E}lectrolytes: {A}n {I}n {S}itu {ESEMS}tudy},
      journal      = {Crystal growth $\&$ design},
      volume       = {23},
      issn         = {1528-7483},
      address      = {Washington, DC},
      publisher    = {ACS Publ.},
      reportid     = {FZJ-2023-01909},
      pages        = {1522-1529},
      year         = {2023},
      abstract     = {Solid-state sintering at high temperatures is commonly used
                      to densify solid electrolytes. Yet, optimizing phase purity,
                      structure, and grain sizes of solid electrolytes is
                      challenging due to the lack of understanding of relevant
                      processes during sintering. Here, we use an in situ
                      environmental scanning electron microscopy (ESEM) to monitor
                      the sintering behavior of NASICON-type Li1.3Al0.3Ti1.7(PO4)3
                      (LATP) at low environmental pressures. Our results show that
                      while no major morphological changes are observed at 10–2
                      Pa and only coarsening is induced at 10 Pa, environmental
                      pressures of 300 and 750 Pa lead to the formation of
                      typically sintered LATP electrolytes. Furthermore, the use
                      of pressure as an additional parameter in sintering allows
                      the grain size and shape of electrolyte particles to be
                      controlled.},
      cin          = {IEK-9 / ER-C-2},
      ddc          = {540},
      cid          = {I:(DE-Juel1)IEK-9-20110218 / I:(DE-Juel1)ER-C-2-20170209},
      pnm          = {1223 - Batteries in Application (POF4-122) / 5351 -
                      Platform for Correlative, In Situ and Operando
                      Characterization (POF4-535) / 5353 - Understanding the
                      Structural and Functional Behavior of Solid State Systems
                      (POF4-535) / Electroscopy - Electrochemistry of
                      All-solid-state-battery Processes using Operando Electron
                      Microscopy (892916)},
      pid          = {G:(DE-HGF)POF4-1223 / G:(DE-HGF)POF4-5351 /
                      G:(DE-HGF)POF4-5353 / G:(EU-Grant)892916},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {36879774},
      UT           = {WOS:000942872900001},
      doi          = {10.1021/acs.cgd.2c01098},
      url          = {https://juser.fz-juelich.de/record/1006877},
}