001008574 001__ 1008574
001008574 005__ 20240708133922.0
001008574 037__ $$aFZJ-2023-02407
001008574 041__ $$aEnglish
001008574 1001_ $$0P:(DE-Juel1)190476$$aDiaz Gomez, Laura Johana$$b0$$eCorresponding author$$ufzj
001008574 1112_ $$aIEK-6 Institutsseminar$$wGermany
001008574 245__ $$aPreliminary extraction and characterization studies of water-soluble octa carboxylic acids for the separation of trivalent actinides$$f2023-06-14 -
001008574 260__ $$c2023
001008574 3367_ $$033$$2EndNote$$aConference Paper
001008574 3367_ $$2DataCite$$aOther
001008574 3367_ $$2BibTeX$$aINPROCEEDINGS
001008574 3367_ $$2ORCID$$aLECTURE_SPEECH
001008574 3367_ $$0PUB:(DE-HGF)31$$2PUB:(DE-HGF)$$aTalk (non-conference)$$btalk$$mtalk$$s1688375652_3072$$xOther
001008574 3367_ $$2DINI$$aOther
001008574 520__ $$aSeparation of An and Ln is an important part in the recycling process of nuclear fuel. Therefore, many ligands have been tested over the years and several separation processes have successfully been demonstrated on the laboratory scale (e.g., AmSel, SANEX, DIAMEX). Current research aims at the development of new ligands which are built only with carbon, hydrogen, oxygen, and nitrogen (CHON), because they can be incinerated completely withoutsecondary waste production. Within the BMUV funded SEPAM project, we tested new water-soluble ligands for the selective separation of Am(III) and Cm(III) from the trivalent Ln. These ligands have the characteristic of having eight carboxylic acid groups in the outer peripheryand differ in the central core, where the metal ion complexation occurs (pyridine, bipyridine and phenanthroline, Figure 1). These ligands might act as CHON alternatives to the sulphonated aqueous ligands used in the i- SANEX1 and AmSel2 systems (SO3-Ph-BTP, SO3-Ph-BTBP1 and AmSel2 systems (SO3-Ph-BTP, SO3-Ph-BTBP) We present results of extraction studies using the three ligands. 2,6-Bis [5,6-di(3,4-dicarboxyphenyl)-1,2,4-triazin-3-yl] pyridine (BTP-octa-COOH) showed the best results with good separation factors for Eu/Am. Therefore, BTP-octa-COOH might be an interesting new hydrophilic complexant and CHON-alternative to SO3-Ph-BTP in the i-SANEX system. The complexation of the ligand with 248Cm(III) and Eu(III) was studied using t ime resolved laser-induced spectroscopy (TRLFS) in HClO4 and HNO3 to determine the stability constants of each formed species. We present and discuss the results of extraction and TRLFS experiments. Funding for this research was provided by the Federal Ministry for the Environment, Nature Conservation, Nuclear Safety and Consumer Protection, project SEPAM (02E11921A).
001008574 536__ $$0G:(DE-HGF)POF4-1412$$a1412 - Predisposal (POF4-141)$$cPOF4-141$$fPOF IV$$x0
001008574 536__ $$0G:(BMWi)02E11921A$$aVerbundprojekt: Untersuchungen zur SEParation von AMericium aus hochradioaktiven Abfalllösungen (SEPAM), Teilprojekt A (02E11921A)$$c02E11921A$$x1
001008574 7001_ $$0P:(DE-HGF)0$$aWeßling, Patrik$$b1
001008574 7001_ $$0P:(DE-Juel1)130438$$aWilden, Andreas$$b2$$ufzj
001008574 7001_ $$0P:(DE-Juel1)130383$$aModolo, Giuseppe$$b3$$ufzj
001008574 909CO $$ooai:juser.fz-juelich.de:1008574$$pVDB
001008574 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)190476$$aForschungszentrum Jülich$$b0$$kFZJ
001008574 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)130438$$aForschungszentrum Jülich$$b2$$kFZJ
001008574 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)130383$$aForschungszentrum Jülich$$b3$$kFZJ
001008574 9131_ $$0G:(DE-HGF)POF4-141$$1G:(DE-HGF)POF4-140$$2G:(DE-HGF)POF4-100$$3G:(DE-HGF)POF4$$4G:(DE-HGF)POF$$9G:(DE-HGF)POF4-1412$$aDE-HGF$$bForschungsbereich Energie$$lNukleare Entsorgung, Sicherheit und Strahlenforschung (NUSAFE II)$$vNukleare Entsorgung$$x0
001008574 9141_ $$y2023
001008574 920__ $$lyes
001008574 9201_ $$0I:(DE-Juel1)IEK-6-20101013$$kIEK-6$$lNukleare Entsorgung$$x0
001008574 980__ $$atalk
001008574 980__ $$aVDB
001008574 980__ $$aI:(DE-Juel1)IEK-6-20101013
001008574 980__ $$aUNRESTRICTED
001008574 981__ $$aI:(DE-Juel1)IFN-2-20101013