001017530 001__ 1017530
001017530 005__ 20240711085552.0
001017530 0247_ $$2doi$$a10.1093/jmicro/dfac064
001017530 0247_ $$2ISSN$$a2050-5698
001017530 0247_ $$2ISSN$$a0022-0744
001017530 0247_ $$2ISSN$$a1477-9986
001017530 0247_ $$2ISSN$$a2050-5701
001017530 0247_ $$2datacite_doi$$a10.34734/FZJ-2023-04179
001017530 0247_ $$2pmid$$a36408996
001017530 0247_ $$2WOS$$aWOS:000898442800001
001017530 037__ $$aFZJ-2023-04179
001017530 082__ $$a530
001017530 1001_ $$0P:(DE-HGF)0$$aDing, Ziming$$b0
001017530 245__ $$aExploring the influence of focused ion beam processing and scanning electron microscopy imaging on solid-state electrolytes
001017530 260__ $$aTokyo$$bOxford Univ. Press$$c2023
001017530 3367_ $$2DRIVER$$aarticle
001017530 3367_ $$2DataCite$$aOutput Types/Journal article
001017530 3367_ $$0PUB:(DE-HGF)16$$2PUB:(DE-HGF)$$aJournal Article$$bjournal$$mjournal$$s1700033191_8819
001017530 3367_ $$2BibTeX$$aARTICLE
001017530 3367_ $$2ORCID$$aJOURNAL_ARTICLE
001017530 3367_ $$00$$2EndNote$$aJournal Article
001017530 520__ $$aPerforming reliable preparation of transmission electron microscopy (TEM) samples is the necessary basis for a meaningful investigation by ex situ and even more so by in situ TEM techniques, but it is challenging using materials that are sensitive to electron beam irradiation. Focused ion beam is currently the most commonly employed technique for a targeted preparation, but the structural modifications induced during focused ion beam preparation are not fully understood for a number of materials. Here, we have investigated the impact of both the electron and the Ga+ ion beam on insulating solid-state electrolytes (lithium phosphorus oxynitride, Na-β"-alumina solid electrolyte and Na3.4Si2.4Zr2P0.6O12 (NaSICON)) and observed significant lithium/sodium whisker growth induced by both the electron and ion beam already at fairly low dose, leading to a significant change in the chemical composition. The metal whisker growth is presumably mainly due to surface charging, which can be reduced by coating with a gold layer or preparation under cryogenic conditions as efficient approaches to stabilize the solid electrolyte for scanning electron microscopy imaging and TEM sample preparation. Details on the different preparation approaches, the acceleration voltage dependence and the induced chemical and morphological changes are reported.
001017530 536__ $$0G:(DE-HGF)POF4-1221$$a1221 - Fundamentals and Materials (POF4-122)$$cPOF4-122$$fPOF IV$$x0
001017530 588__ $$aDataset connected to CrossRef, Journals: juser.fz-juelich.de
001017530 7001_ $$0P:(DE-HGF)0$$aTang, Yushu$$b1
001017530 7001_ $$0P:(DE-HGF)0$$aChakravadhanula, Venkata Sai Kiran$$b2
001017530 7001_ $$0P:(DE-Juel1)129628$$aMa, Qianli$$b3$$ufzj
001017530 7001_ $$0P:(DE-Juel1)129667$$aTietz, Frank$$b4$$ufzj
001017530 7001_ $$0P:(DE-HGF)0$$aDai, Yuting$$b5
001017530 7001_ $$0P:(DE-HGF)0$$aScherer, Torsten$$b6
001017530 7001_ $$0P:(DE-HGF)0$$aKübel, Christian$$b7$$eCorresponding author
001017530 773__ $$0PERI:(DE-600)2708387-1$$a10.1093/jmicro/dfac064$$gVol. 72, no. 4, p. 326 - 335$$n4$$p326 - 335$$tMicroscopy$$v72$$x2050-5698$$y2023
001017530 8564_ $$uhttps://juser.fz-juelich.de/record/1017530/files/dfac064.pdf$$yOpenAccess
001017530 909CO $$ooai:juser.fz-juelich.de:1017530$$pdnbdelivery$$pdriver$$pVDB$$popen_access$$popenaire
001017530 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)129628$$aForschungszentrum Jülich$$b3$$kFZJ
001017530 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)129667$$aForschungszentrum Jülich$$b4$$kFZJ
001017530 9101_ $$0I:(DE-HGF)0$$6P:(DE-HGF)0$$aExternal Institute$$b7$$kExtern
001017530 9131_ $$0G:(DE-HGF)POF4-122$$1G:(DE-HGF)POF4-120$$2G:(DE-HGF)POF4-100$$3G:(DE-HGF)POF4$$4G:(DE-HGF)POF$$9G:(DE-HGF)POF4-1221$$aDE-HGF$$bForschungsbereich Energie$$lMaterialien und Technologien für die Energiewende (MTET)$$vElektrochemische Energiespeicherung$$x0
001017530 9141_ $$y2023
001017530 915__ $$0LIC:(DE-HGF)CCBY4$$2HGFVOC$$aCreative Commons Attribution CC BY 4.0
001017530 915__ $$0StatID:(DE-HGF)0200$$2StatID$$aDBCoverage$$bSCOPUS$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)0160$$2StatID$$aDBCoverage$$bEssential Science Indicators$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)1050$$2StatID$$aDBCoverage$$bBIOSIS Previews$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)1190$$2StatID$$aDBCoverage$$bBiological Abstracts$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)0600$$2StatID$$aDBCoverage$$bEbsco Academic Search$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)1040$$2StatID$$aDBCoverage$$bZoological Record$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)0100$$2StatID$$aJCR$$bMICROSCOPY-JPN : 2022$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)0113$$2StatID$$aWoS$$bScience Citation Index Expanded$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)1030$$2StatID$$aDBCoverage$$bCurrent Contents - Life Sciences$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)0150$$2StatID$$aDBCoverage$$bWeb of Science Core Collection$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)9900$$2StatID$$aIF < 5$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)0510$$2StatID$$aOpenAccess
001017530 915__ $$0StatID:(DE-HGF)0030$$2StatID$$aPeer Review$$bASC$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)0300$$2StatID$$aDBCoverage$$bMedline$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)0320$$2StatID$$aDBCoverage$$bPubMed Central$$d2023-08-28
001017530 915__ $$0StatID:(DE-HGF)0420$$2StatID$$aNationallizenz$$d2023-08-28$$wger
001017530 915__ $$0StatID:(DE-HGF)0199$$2StatID$$aDBCoverage$$bClarivate Analytics Master Journal List$$d2023-08-28
001017530 920__ $$lyes
001017530 9201_ $$0I:(DE-Juel1)IEK-1-20101013$$kIEK-1$$lWerkstoffsynthese und Herstellungsverfahren$$x0
001017530 9801_ $$aFullTexts
001017530 980__ $$ajournal
001017530 980__ $$aVDB
001017530 980__ $$aUNRESTRICTED
001017530 980__ $$aI:(DE-Juel1)IEK-1-20101013
001017530 981__ $$aI:(DE-Juel1)IMD-2-20101013