Hauptseite > Publikationsdatenbank > Monoclinic symmetry of the hcp-type ordered areas in bulk cobalt > print

001     1018231
005     20231213115707.0
024 7 _ |a 10.1103/PhysRevB.107.104104
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024 7 _ |a 10.34734/FZJ-2023-04627
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041 _ _ |a English
082 _ _ |a 530
100 1 _ |a Kozłowski, Paweł
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245 _ _ |a Monoclinic symmetry of the hcp-type ordered areas in bulk cobalt
260 _ _ |a College Park, Maryland
|c 2023
|b Americal Physical Society
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520 _ _ |a The gradual ferromagnetic spin reorientation in hexagonal close packed cobalt (hcp-Co) phase between 230 $^\circ$C and 330 $^\circ$C reported for a Co single crystal [Bertaut $\textit{et al.}$, Solid State Commun. $\textbf{1}$, 81 (1963)] suggests that this phase could not have a hexagonal symmetry. This hypothesis is verified positively by synchrotron radiation diffraction and neutron diffraction on polycrystalline powder cobalt. The analysis of diffraction data has been done by using a specific set of Bragg peaks, which are not sensitive to the stacking faults present in abundance in hcp-Co. The crystal structure of the hcp-type ordered areas of cobalt is described by the monoclinic symmetry with the magnetic space group $C2'/m'$. In this monoclinic crystal structure the former hexagonal $[001]$ axis is no longer perpendicular to the hexagonal layers. The hexagonal $[001]$ and $[010]$ axes make an angle equal $\alpha \approx 90.10(1)$ $^\circ$, while the angle between in-plane $[100]$ and $[010]$ axes equals $\gamma \approx 120.11(1)$ $^\circ$. The monoclinic symmetry provides an approximate description of the crystal structure of the stacking faulted hcp-Co areas coexisting with fcc-Co areas.
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700 1 _ |a Fabrykiewicz, Piotr
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700 1 _ |a Sosnowska, Izabela
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700 1 _ |a Przeniosło, Radosław
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