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@INPROCEEDINGS{Durmus:1020596,
author = {Durmus, Yasin Emre and Montiel Guerrero, Saul Said and
Dzieciol, Krzysztof and Kungl, Hans and Tempel, Hermann and
Eichel, Rüdiger-A.},
title = {{I}mproved {E}lectrochemical {P}erformance of {Z}inc
{A}nodes by {E}lectrolyte {A}dditives in {N}ear-{N}eu-tral
{Z}inc-{A}ir {B}atteries},
reportid = {FZJ-2024-00291},
year = {2023},
abstract = {Metal-air batteries are considered up-and-coming
electrochemical energy storage technolo-gies due to
possessing very high theoretical energy densities while
utilizing cost-effective, safe, and abundant materials.
Among various possible configurations, zinc-based metal-air
batteries are one of the most advanced for primary and
secondary applications. Although primary Zinc-air batteries
(ZABs) have been commercially available for various
applications, secondary bat-teries have faced challenges,
especially in alkaline media. In this regard, employing
aqueous neutral electrolytes brings several advantages, such
as suppressed carbonization of the elec-trolyte and dendrite
formation. However, the performance of such ZABs with
neutral electro-lytes can be hindered by the passivation of
the zinc surface, the formation of insoluble zinc species,
and corrosion.The objective of the present work is to
evaluate the influence of Ethylenediaminetetraacetic acid
(EDTA) electrolyte additive on the performance of
near-neutral secondary Zn-air batteries. The electrochemical
behaviour of Zn electrodes was investigated in 2M NaCl (pH
10) solutions with and without EDTA additive. Initially,
open-circuit and potentiodynamic polarization exper-iments
were conducted to extract the corrosion parameters of the Zn
electrodes. The interme-diate-term (24 h) discharge
experiments were performed under current densities of 0.1,
0.25, 0.5, and 1 mA/cm2 in a three-electrode half-cell
setup. These electrochemical measurements confirmed that Zn
is only partially active in neat 2M NaCl electrolytes.
However, it could still be discharged up to 1 mA/cm2 at
discharge potentials around −1.0 VAg/AgCl. In order to
study the dissolution behaviour and the discharge products,
the surface of the electrodes was further characterized by a
laser scanning microscope (LSM), X-ray diffraction (XRD),
and scanning electron microscope (SEM) upon discharge
experiments. The performance of full-cell Zn-air batteries
was then evaluated in galvanostatic discharge experiments
(in primary-mode) up to 930 h with specific energies up to
840 Wh/kgZn and in galvanostatic cycling experiments (in
secondary mode) up to 575 h with 70 cycles. In comparison to
neat electrolytes, the addition of EDTA to the electrolyte
results in enhanced specific energies and mass utilization
efficien-cies of near-neutral zinc-air batteries.},
month = {Sep},
date = {2023-09-18},
organization = {3RD INTERNATIONAL ZINC-AIR AND OTHER
ZINC BATTERIES WORKSHOP, Ulm (Germany),
18 Sep 2023 - 19 Sep 2023},
subtyp = {After Call},
cin = {IEK-9},
cid = {I:(DE-Juel1)IEK-9-20110218},
pnm = {1223 - Batteries in Application (POF4-122)},
pid = {G:(DE-HGF)POF4-1223},
typ = {PUB:(DE-HGF)24},
url = {https://juser.fz-juelich.de/record/1020596},
}