001021028 001__ 1021028 001021028 005__ 20240709082106.0 001021028 037__ $$aFZJ-2024-00488 001021028 1001_ $$0P:(DE-Juel1)180432$$aBasak, Shibabrata$$b0$$eCorresponding author 001021028 1112_ $$aThe 20th of International Microscopy Congress$$cBusan$$d2023-09-10 - 2023-09-15$$gICM20$$wSouth Korea 001021028 245__ $$aStudying Electrochemistry using Liquid Phase TEM 001021028 260__ $$c2023 001021028 3367_ $$033$$2EndNote$$aConference Paper 001021028 3367_ $$2DataCite$$aOther 001021028 3367_ $$2BibTeX$$aINPROCEEDINGS 001021028 3367_ $$2DRIVER$$aconferenceObject 001021028 3367_ $$2ORCID$$aLECTURE_SPEECH 001021028 3367_ $$0PUB:(DE-HGF)6$$2PUB:(DE-HGF)$$aConference Presentation$$bconf$$mconf$$s1705297033_12154$$xAfter Call 001021028 520__ $$aIn recent years, in-situ liquid-phase transmission electron microscopy (LPTEM) has emerged as a powerful technique for investigating the dynamic electrochemical processes that occur in electrochemical storage and conversion systems. However, to obtain accurate and reliable results, it is essential that the chemical environment within the TEM can be precisely controlled in a reproducible manner so that the nucleation and growth of lithium or zinc or the conversion of CO2 at the electrocatalysts can be studied under realistic conditions. Additionally, the system should enable obtaining high-quality imaging and analytical information to gain valuable insights into the underlying mechanisms that govern these complex systems.Smart micro electrical mechanical systems (MEMS) and holder designs have enabled us to control liquid flow and thickness, allowing us to create a stable and reproducible environment that is ideal for investigating the electrochemical processes of interest. This has also enabled us to obtain structural, and chemical information that reveals details about the electrochemical processes using 4DSTEM, EDX, EELS. Furthermore, the use of image processing has allowed us to extract detailed information from the experimental data sets, taking the first steps toward quantification. This advance in LPTEM provides the pathway to developing new and more efficient energy technologies that can help to address the global energy challenges. 001021028 536__ $$0G:(DE-HGF)POF4-1232$$a1232 - Power-based Fuels and Chemicals (POF4-123)$$cPOF4-123$$fPOF IV$$x0 001021028 7001_ $$0P:(DE-Juel1)180853$$aPark, Junbeom$$b1 001021028 7001_ $$0P:(DE-HGF)0$$aSun, Hongyu$$b2 001021028 7001_ $$0P:(DE-Juel1)156123$$aEichel, Rüdiger-A.$$b3$$ufzj 001021028 909CO $$ooai:juser.fz-juelich.de:1021028$$pVDB 001021028 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)180432$$aForschungszentrum Jülich$$b0$$kFZJ 001021028 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)180853$$aForschungszentrum Jülich$$b1$$kFZJ 001021028 9101_ $$0I:(DE-HGF)0$$6P:(DE-HGF)0$$aDENSSolutions B.V., Netherlands$$b2 001021028 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)156123$$aForschungszentrum Jülich$$b3$$kFZJ 001021028 9101_ $$0I:(DE-588b)36225-6$$6P:(DE-Juel1)156123$$aRWTH Aachen$$b3$$kRWTH 001021028 9131_ $$0G:(DE-HGF)POF4-123$$1G:(DE-HGF)POF4-120$$2G:(DE-HGF)POF4-100$$3G:(DE-HGF)POF4$$4G:(DE-HGF)POF$$9G:(DE-HGF)POF4-1232$$aDE-HGF$$bForschungsbereich Energie$$lMaterialien und Technologien für die Energiewende (MTET)$$vChemische Energieträger$$x0 001021028 9141_ $$y2023 001021028 920__ $$lyes 001021028 9201_ $$0I:(DE-Juel1)IEK-9-20110218$$kIEK-9$$lGrundlagen der Elektrochemie$$x0 001021028 980__ $$aconf 001021028 980__ $$aVDB 001021028 980__ $$aI:(DE-Juel1)IEK-9-20110218 001021028 980__ $$aUNRESTRICTED 001021028 981__ $$aI:(DE-Juel1)IET-1-20110218