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@INPROCEEDINGS{Basak:1021028,
      author       = {Basak, Shibabrata and Park, Junbeom and Sun, Hongyu and
                      Eichel, Rüdiger-A.},
      title        = {{S}tudying {E}lectrochemistry using {L}iquid {P}hase {TEM}},
      reportid     = {FZJ-2024-00488},
      year         = {2023},
      abstract     = {In recent years, in-situ liquid-phase transmission electron
                      microscopy (LPTEM) has emerged as a powerful technique for
                      investigating the dynamic electrochemical processes that
                      occur in electrochemical storage and conversion systems.
                      However, to obtain accurate and reliable results, it is
                      essential that the chemical environment within the TEM can
                      be precisely controlled in a reproducible manner so that the
                      nucleation and growth of lithium or zinc or the conversion
                      of CO2 at the electrocatalysts can be studied under
                      realistic conditions. Additionally, the system should enable
                      obtaining high-quality imaging and analytical information to
                      gain valuable insights into the underlying mechanisms that
                      govern these complex systems.Smart micro electrical
                      mechanical systems (MEMS) and holder designs have enabled us
                      to control liquid flow and thickness, allowing us to create
                      a stable and reproducible environment that is ideal for
                      investigating the electrochemical processes of interest.
                      This has also enabled us to obtain structural, and chemical
                      information that reveals details about the electrochemical
                      processes using 4DSTEM, EDX, EELS. Furthermore, the use of
                      image processing has allowed us to extract detailed
                      information from the experimental data sets, taking the
                      first steps toward quantification. This advance in LPTEM
                      provides the pathway to developing new and more efficient
                      energy technologies that can help to address the global
                      energy challenges.},
      month         = {Sep},
      date          = {2023-09-10},
      organization  = {The 20th of International Microscopy
                       Congress, Busan (South Korea), 10 Sep
                       2023 - 15 Sep 2023},
      subtyp        = {After Call},
      cin          = {IEK-9},
      cid          = {I:(DE-Juel1)IEK-9-20110218},
      pnm          = {1232 - Power-based Fuels and Chemicals (POF4-123)},
      pid          = {G:(DE-HGF)POF4-1232},
      typ          = {PUB:(DE-HGF)6},
      url          = {https://juser.fz-juelich.de/record/1021028},
}