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@ARTICLE{Helmers:1024752,
author = {Helmers, Laura and Frankenberg, Finn and Brokmann, Julian
and Burmeister, Christine and Buchheit, Annika and Kwade,
Arno and Michalowski, Peter},
title = {{F}unctionalized {T}hiophosphate and {O}xidic {F}iller
{P}articles for {H}ybrid {S}olid {E}lectrolytes},
journal = {ChemElectroChem},
volume = {10},
number = {21},
issn = {2196-0216},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2024-02418},
pages = {e202300310},
year = {2023},
note = {Unterstützt durch: BMBF 3XP0202F (3D-SSB) $\&$ BMBF
03XP0432A (FB2-Prod)},
abstract = {To achieve the commercialization of solid-state-batteries
(SSBs), solid electrolyte properties need to be further
improved. The hybrid solid electrolyte (HSE) approach is
expected to combine the favorable properties of different
solid electrolyte classes and is therefore systematically
investigated. Mixing low amounts of thiophosphate or oxide
filler particles (FP) into a polyethylene oxide (PEO)
polyethylene glycol (PEG) and lithium salt
bis(trifluoromethane)sulfonimide (LiTFSI) matrix cannot
improve the electrochemical properties. Silanization of the
thiophosphate FPs significantly increases the ionic
conductivity to 0.1 mS cm−1 at room temperature
compared to 0.017 mS cm−1 for a pure PEO solid
electrolyte. Moreover, a correlation between the intrinsic
conductivity of the FPs and the resulting conductivity of
the HSE is observed. Also, the functionalization is
successfully transferred to oxide FPs. In addition to an
equally significant increase in ionic conductivity, a strong
influence of the crystallite size of the FPs on the
resulting ionic conductivity of the HSE was found. The
discovered effect of FP surface structure on overall HSE
conductivity indicates a participation of the FP surface in
ion transport and emphasizes the need for tailored filler
design in HSE applications.},
cin = {IEK-12},
ddc = {540},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {1221 - Fundamentals and Materials (POF4-122)},
pid = {G:(DE-HGF)POF4-1221},
typ = {PUB:(DE-HGF)16},
UT = {WOS:001085756300001},
doi = {10.1002/celc.202300310},
url = {https://juser.fz-juelich.de/record/1024752},
}