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001025009 1001_ $$00000-0002-1670-1798$$aWrogemann, Jens Matthies$$b0$$eCorresponding author
001025009 245__ $$aOvercoming Diffusion Limitation of Faradaic Processes: Property‐Performance Relationships of 2D Conductive Metal‐Organic Framework Cu 3 (HHTP) 2 for Reversible Lithium‐Ion Storage
001025009 260__ $$aWeinheim$$bWiley-VCH$$c2023
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001025009 520__ $$aFaradaic reactions including charge transfer are often accompanied with diffusion limitation inside the bulk. Conductive two-dimensional frameworks (2D MOFs) with a fast ion transport can combine both—charge transfer and fast diffusion inside their porous structure. To study remaining diffusion limitations caused by particle morphology, different synthesis routes of Cu-2,3,6,7,10,11-hexahydroxytriphenylene (Cu3(HHTP)2), a copper-based 2D MOF, are used to obtain flake- and rod-like MOF particles. Both morphologies are systematically characterized and evaluated for redox-active Li+ ion storage. The redox mechanism is investigated by means of X-ray absorption spectroscopy, FTIR spectroscopy and in situ XRD. Both types are compared regarding kinetic properties for Li+ ion storage via cyclic voltammetry and impedance spectroscopy. A significant influence of particle morphology for 2D MOFs on kinetic aspects of electrochemical Li+ ion storage can be observed. This study opens the path for optimization of redox active porous structures to overcome diffusion limitations of Faradaic processes.
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001025009 7001_ $$aLüther, Marco Joes$$b1
001025009 7001_ $$aBärmann, Peer$$b2
001025009 7001_ $$aLounasvuori, Mailis$$b3
001025009 7001_ $$aJaved, Ali$$b4
001025009 7001_ $$0P:(DE-HGF)0$$aTiemann, Michael$$b5
001025009 7001_ $$0P:(DE-HGF)0$$aGolnak, Ronny$$b6
001025009 7001_ $$0P:(DE-HGF)0$$aXiao, Jie$$b7
001025009 7001_ $$aPetit, Tristan$$b8
001025009 7001_ $$0P:(DE-HGF)0$$aPlacke, Tobias$$b9
001025009 7001_ $$0P:(DE-Juel1)166130$$aWinter, Martin$$b10$$ufzj
001025009 773__ $$0PERI:(DE-600)2011836-3$$a10.1002/anie.202303111$$gVol. 62, no. 26, p. e202303111$$n26$$pe202303111$$tAngewandte Chemie$$v62$$x1433-7851$$y2023
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