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001025011 1001_ $$aYing, Bixian$$b0
001025011 245__ $$aMonitoring the Formation of Nickel-Poor and Nickel-Rich Oxide Cathode Materials for Lithium-Ion Batteries with Synchrotron Radiation
001025011 260__ $$aWashington, DC$$bAmerican Chemical Society$$c2023
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001025011 520__ $$aThe syntheses of Ni-poor (NCM111, LiNi1/3Co1/3Mn1/3O2) and Ni-rich (NCM811 LiNi0.8Co0.1Mn0.1O2) lithium transition-metal oxides (space group R3̅m) from hydroxide precursors (Ni1/3Co1/3Mn1/3(OH)2, Ni0.8Co0.1Mn0.1(OH)2) are investigated using in situ synchrotron powder diffraction and near-edge X-ray absorption fine structure spectroscopy. The development of the layered structure of these two cathode materials proceeds via two utterly different reaction mechanisms. While the synthesis of NCM811 involves a rock salt-type intermediate phase, NCM111 reveals a layered structure throughout the entire synthesis. Moreover, the necessity and the impact of a preannealing step and a high-temperature holding step are discussed.
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001025011 7001_ $$00000-0003-4704-9242$$aFitzpatrick, Jack R.$$b1
001025011 7001_ $$aTeng, Zhenjie$$b2
001025011 7001_ $$aChen, Tianxiang$$b3
001025011 7001_ $$aLo, Tsz Woon Benedict$$b4
001025011 7001_ $$aSiozios, Vassilios$$b5
001025011 7001_ $$00000-0002-8306-3634$$aMurray, Claire A.$$b6
001025011 7001_ $$aBrand, Helen E. A.$$b7
001025011 7001_ $$aDay, Sarah$$b8
001025011 7001_ $$aTang, Chiu C.$$b9
001025011 7001_ $$00000-0002-3993-9045$$aWeatherup, Robert S.$$b10
001025011 7001_ $$00000-0002-7346-7176$$aMerz, Michael$$b11
001025011 7001_ $$0P:(DE-HGF)0$$aNagel, Peter$$b12
001025011 7001_ $$0P:(DE-HGF)0$$aSchuppler, Stefan$$b13
001025011 7001_ $$0P:(DE-Juel1)166130$$aWinter, Martin$$b14$$ufzj
001025011 7001_ $$00000-0003-0203-440X$$aKleiner, Karin$$b15$$eCorresponding author
001025011 773__ $$0PERI:(DE-600)1500399-1$$a10.1021/acs.chemmater.2c02639$$gVol. 35, no. 4, p. 1514 - 1526$$n4$$p1514 - 1526$$tChemistry of materials$$v35$$x0897-4756$$y2023
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