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@ARTICLE{VargasBarbosa:1025083,
author = {Vargas-Barbosa, Nella Marie and Puls, Sebastian and
Woolley, Henry Michael},
title = {{H}ybrid {M}aterial {C}oncepts for {T}hiophosphate-{B}ased
{S}olid-{S}tate {B}atteries},
journal = {Meeting abstracts},
volume = {MA2023-01},
number = {6},
issn = {1091-8213},
address = {Pennington, NJ},
publisher = {Soc.},
reportid = {FZJ-2024-02671},
pages = {984 - 984},
year = {2023},
note = {Hierbei handelt es sich lediglich um einen Abstract.},
abstract = {Solid-state batteries (SSBs) could replace conventional
lithium-ion batteries due to the possibility of increasing
the energy density of the cells by using lithium metal as
the anode material.[1] Among the many electrolyte candidates
for lithium SSBs, the lithium thiophosphates are
particularly interesting due to their high ionic
conductivities at room temperature (>1 mS/cm). However, the
(electro)chemical stability of these solid electrolytes is
limited and not fully compatible with state-of-the-art
high-potential cathode active materials[2] or the lithium
metal anode.[3] At the cell level, the formation of
interparticle voids between the various battery components
(solid electrolyte, cathode active material, anode material,
additives, decomposition interphases) hinder the net
transport during cycling. To address the latter
electro-chemo-mechanical challenges, we are exploring hybrid
material approaches, in which we combine established
materials (solid electrolytes, liquid electrolytes and/or
polymer additives) with state-of-the-art cathode active
materials and test their electrochemical performance in
solid-state battery (half-)cells. Such cycling results are
complimented by detailed electrochemical transport studies
in symmetrical cells using DC polarization and
electrochemical impedance spectroscopy, including
transmission-line modeling. ex.situ chemically-specific
spectroscopic methods are used to support our hypotheses and
interpretation of the electrochemical results. Taken
together, we attain a better picture on the positive (or
negative) role hybrid materials play in SSBs. In this talk,
we will showcase two hybrid systems, namely ionic
liquid/thiophosphate lithium hybrid electrolytes and
conductive polymers additives in NMC-based catholyte
composites for Li6PS5Cl cells. The first part of the talk we
will discuss the results in which we evaluate the
performance of liquid electrolyte-solid electrolyte
materials against lithium metal using galvanostatic
electrochemical impedance spectroscopy. In the second part,
we elucidate the partial ionic and electronic transport in
polymer electrolyte-Li6PS5Cl-NMC catholytes as a function of
polymer content using impedance spectroscopy and its effect
in the cycling performance, both the stability as well as
the magnitude of the discharge capacities. These systems
serve as a good starting point for the further development
and incorporation of hybrid materials in SSBs.Literature:
[1] W. G. Zeier and J. Janek Nature Energy, 2016, 1, 16141.
[2] G.F. Dewald, S. Ohno, M.A. Kraft, R. Kroever, P. Till,
N.M. Vargas-Barbosa, J. Janek, W.G. Zeier Chem. Mater. 2019,
31, 8328. [3] L. M. Riegger, R. Schlem, J. Sann, W. G.
Zeier, J. Janek, Angew. Chem. Int Ed 2021, 60, 6718.},
cin = {IEK-12},
ddc = {540},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {1221 - Fundamentals and Materials (POF4-122)},
pid = {G:(DE-HGF)POF4-1221},
typ = {PUB:(DE-HGF)16},
doi = {10.1149/MA2023-016984mtgabs},
url = {https://juser.fz-juelich.de/record/1025083},
}