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@ARTICLE{Wellmann:1025203,
author = {Wellmann, Peter and Strüber, Sven and Steiner, Johannes
and Ihle, Jonas and Schultheiss, Jana and Nguyen, Binh Duong
and Sandfeld, Stefan and Salamon, Michael and Uhlmann,
Norman},
title = {({I}nvited) {A}pplication of 3{D} in-{S}itu {X}-{R}ay
{V}isualization to {T}rack the {F}ormation of {D}islocation
{C}lusters during {PVT} {G}rowth of {S}i{C}},
journal = {Meeting abstracts},
volume = {MA2023-02},
number = {35},
issn = {1091-8213},
address = {Pennington, NJ},
publisher = {Soc.},
reportid = {FZJ-2024-02771},
pages = {1693 - 1693},
year = {2023},
abstract = {SiC has become the key player among wide bandgap
semiconductors for power electronic applications. Since the
first description of the physical vapour transport (PVT)
growth process of SiC by Tairov and Tsvetkov (J. Crystal
Growth, 43, 209(1978)), there has been steady progress in
SiC-based crystal growth, epitaxy and device processing. The
success of SiC compared to Si is related to its superior
material properties such as extremely high electrical
breakdown field and high thermal conductivity compared to
the standard silicon counterpart. In addition, SiC device
processing utilises much of the standard Si processing
equipment. A major reason for the success of SiC in power
electronic applications compared to other wide bandgap
counterparts such as GaN, Ga2O3 and diamond is related to
the availability of large diameter SiC wafer materials
(150mm = standard, 200mm = developped). Bulk SiC growth is
now a very well developed process with comparatively high
yields. The extraordinary physical properties also include
obstacles related to the strong chemical bonding and complex
phase diagram of the material, which pose challenges to the
growth process. Therefore, there are still a number of open
questions related to the nucleation, progression and
termination of the bulk growth process that require
fundamental research in materials science and technology.The
aim of this presentation is (i) to give an overview of the
state-of-the-art PVT growth process and (ii) to discuss a
current research topic dealing with the early stage of the
growth process and the defect formation that can occur
during the initial nucleation of SiC. We have applied 3D
in-situ visualisation of the growth process using X-ray
computed tomography to visualise island formation on the
large seeding area. These data are related to growth process
instabilities such as temperature variations during the
seeding process and axial doping level changes from the seed
to the newly grown crystal. Both process instabilities
induce mechanical stress on the SiC lattice and act as
sources for dislocation generation and multiplication. We
will show a series of growth processes with varying growth
parameters that shed light on the initial growth stage of
SiC.As the crystal diameter of SiC increases from 150 mm to
200 mm, the results of this study become increasingly
important.},
cin = {IAS-9},
ddc = {540},
cid = {I:(DE-Juel1)IAS-9-20201008},
pnm = {5111 - Domain-Specific Simulation $\&$ Data Life Cycle Labs
(SDLs) and Research Groups (POF4-511)},
pid = {G:(DE-HGF)POF4-5111},
typ = {PUB:(DE-HGF)16},
doi = {10.1149/MA2023-02351693mtgabs},
url = {https://juser.fz-juelich.de/record/1025203},
}