%0 Journal Article %A Ünal, Leyla %A Maccio-Figgemeier, Viviane %A Gebresilassie Eshetu, Gebrekidan %A Figgemeier, Egbert %T In‐Vitro Electrochemical Prelithiation: A Key Performance‐Boosting Strategy for Carbon Nanotube‐Containing Silicon‐Based Negative Electrodes in Li‐Ion Batteries %J ChemElectroChem %V 11 %N 17 %@ 2196-0216 %C Weinheim %I Wiley-VCH %M FZJ-2024-03534 %P e202400146 %D 2024 %Z The authors acknowledge the Federal Ministry of Education and Research of Germany (BMBF) for funding this work through the projects, PräLi (03XP0238X) and ProMIZ (13XP0397B). Open-Access funding enabled and organized by Projekt DEAL. %X Prelithiation technology has emerged as an enabling approach towards the practical deployment of Silicon negative electrode-based Li-Ion batteries, leading to significant advancement in initial Coulombic efficiency (ICE), energy density and cycle life. In this study, an electrochemical prelithiation has been applied to Multi-Walled Carbon Nanotubes (MWCNTs)-containing Silicon-rich Silicon/Graphite-based negative electrode, eliminating almost ~51.03 % of its first irreversible capacity losses. In contrast, a benchmarking negative electrode utilizing Carbon black (Super P) as conductive additive is found to demonstrate a reduction of ~39.55 % after prelithiation, which is considerably lower compared to MWCNTs-based electrode system. Post-mortem analysis using Energy-dispersive X-ray (EDX) analysis with a Scanning Electron Microscope (SEM) and Attenuated Total Reflection Fourier Transform Infrared Spectroscopy (ATR-FTIR) shows disparities between pristine-cycled and prelithiated-cycled negative electrodes. Overall, prelithiation enabled MWCNTs can be regarded as an essential additive component in Silicon-based negative electrode systems for high-energy density Li-Ion batteries. %F PUB:(DE-HGF)16 %9 Journal Article %U <Go to ISI:>//WOS:001234783100001 %R 10.1002/celc.202400146 %U https://juser.fz-juelich.de/record/1026942