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@ARTICLE{Lannoye:1028510,
      author       = {Lannoye, Karen De and Belt, Alexander and Reinecke,
                      Ernst-Arndt and Arnold, Lukas},
      title        = {{T}he {T}ube {F}urnace with {O}nline {M}ass {L}oss
                      {M}easurement as a {N}ew {B}ench {S}cale {T}est for
                      {P}yrolysis},
      journal      = {Fire technology},
      volume       = {60},
      issn         = {0015-2684},
      reportid     = {FZJ-2024-04662},
      pages        = {3689-3707},
      year         = {2024},
      abstract     = {In this paper, a new gram scale experiment with well
                      characterised boundary conditions is proposed for pyrolysis
                      experiments. The set-up consists of a tube furnace, based on
                      ISO19700, with a newly designed concept for a balance within
                      the oven, allowing for online mass loss measurements.
                      Samples with a length up to 50 cm can be investigated in
                      this apparatus. The oven allows for experiments at fixed
                      temperatures or at fixed heating rates, under controlled
                      atmosphere, w.r.t. gas composition and flow rate. A thorough
                      characterisation of the set-up is presented, including
                      aspects like reproducibility of the heating rate or the
                      precision of the balance. The functionality of the balance
                      has been demonstrated with calcium carbonate $(CaCO_3)$
                      experiments. This material was chosen because it decomposes
                      in a single reaction, which only releases $CO_2.$ This
                      allows for comparison between the mass loss rate of the
                      balance and the $CO_2$ production rate, measured by a gas
                      analyser. Results for two different heating rates: 3 K/min
                      and 5 K/min and for different masses (25 g and 8.5 g) are
                      presented. The two measurement methods are in excellent
                      agreement. Finally, the data obtained from the new
                      experimental set-up is compared to results from
                      thermogravimetric analyser (TGA) experiments.},
      cin          = {IAS-7 / IET-4},
      ddc          = {620},
      cid          = {I:(DE-Juel1)IAS-7-20180321 / I:(DE-Juel1)IET-4-20191129},
      pnm          = {5111 - Domain-Specific Simulation $\&$ Data Life Cycle Labs
                      (SDLs) and Research Groups (POF4-511) / 1422 - Beyond Design
                      Basis Accidents and Emergency Management (POF4-142)},
      pid          = {G:(DE-HGF)POF4-5111 / G:(DE-HGF)POF4-1422},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:001251071800001},
      doi          = {10.1007/s10694-024-01590-0},
      url          = {https://juser.fz-juelich.de/record/1028510},
}