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@ARTICLE{Scharf:1031177,
author = {Scharf, Felix and Krude, Annalena and Lennartz, Peter and
Clausnitzer, Moritz and Shukla, Gourav and Buchheit, Annika
and Kempe, Fabian and Diddens, Diddo and Glomb, Pascal and
Mitchell, Melanie M. and Danner, Timo and Heuer, Andreas and
Latz, Arnulf and Winter, Martin and Brunklaus, Gunther},
title = {{S}ynergistic {E}nhancement of {M}echanical and
{E}lectrochemical {P}roperties in {G}rafted
{P}olymer/{O}xide {H}ybrid {E}lectrolytes},
journal = {Small},
volume = {20},
number = {47},
issn = {1613-6810},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2024-05581},
pages = {2404537},
year = {2024},
note = {Zudem unterstützt durch: “FB2-Hybrid” (grant:
13XP0428A), “FB2-TheoDat” (grant: 03XP0435A/E).},
abstract = {Lithium metal batteries operated with high voltage cathodes
are predestined for the realization of high energy storage
systems, where solid polymer electrolytes offer a
possibility to improve battery safety. $Al2O3_PCL$ is
introduced as promising hybrid electrolyte made from
polycaprolactone (PCL) and Al2O3 nanoparticles that can be
prepared in a one-pot synthesis as a random mixture of
linear PCL and PCL-grafted Al2O3. Upon grafting, synergistic
effects of mechanical stability and ionic conductivity are
achieved. Due to the mechanical stability, manufacture of
PCL-based membranes with a thickness of 50 µm is feasible,
yielding an ionic conductivity of 5·10−5 S cm−1 at 60
°C. The membrane exhibits an impressive performance of Li
deposition in symmetric Li||Li cells, operating for 1200 h
at a constant and low overvoltage of 54 mV and a current
density of 0.2 mA cm−2. NMC622 | $Al2O3_PCL$ | Li cells
are cycled at rates of up to 1 C, achieving 140 cycles at
$>80\%$ state of health. The straightforward synthesis and
opportunity of upscaling as well as solvent-free
polymerization render the $Al2O3_PCL$ hybrid material as
rather safe, potentially sustainable and affordable
alternative to conventional polymer-based electrolytes.},
cin = {IMD-4},
ddc = {620},
cid = {I:(DE-Juel1)IMD-4-20141217},
pnm = {1221 - Fundamentals and Materials (POF4-122) / FB2-POLY -
Zellplattform Polymere (BMBF-13XP0429A)},
pid = {G:(DE-HGF)POF4-1221 / G:(DE-Juel1)BMBF-13XP0429A},
typ = {PUB:(DE-HGF)16},
pubmed = {39185805},
UT = {WOS:001298262500001},
doi = {10.1002/smll.202404537},
url = {https://juser.fz-juelich.de/record/1031177},
}