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@INPROCEEDINGS{He:1031668,
author = {He, Suqin and Petracic, Oleg and Cao, Lei and Lauter,
Valeria and Zhou, Yunxia and Weber, Moritz and Schubert,
Jürgen and Dittmann, Regina and Waser, R. and Brückel,
Thomas and Gunkel, Felix},
title = {{S}tructural, magnetic and electrical properties of
oxygendeficient{L}a(0.6){S}r(0.4){C}o{O}(3-δ) thin films},
reportid = {FZJ-2024-05778},
year = {2024},
abstract = {Controlled oxygen release or uptake in complex oxides can
induce changes of the crystal structureand simultaneously of
the magnetic and electrical properties. Consequently, a
systematic control ofthe oxygen stoichiometry can enable
potential applications in spintronics, solid oxide fuel
cells andcatalysts. In La0.6Sr0.4CoO3-δ (LSCO) the gradual
oxygen release triggers a phase transition fromthe initial
ferromagnetic (FM) perovskite (PV) structure to an oxygen
vacancy layered antiferromagnetic(AFM) brownmillerite (BM)
structure.We have studied LSCO thin films fabricated by
pulsed laser deposition (PLD). In situ x-ray
diffractionduring thermal annealing reveals the topotactic
phase transition of the LSCO thin films, which can
beattributed to the release of oxygen and ultimately the
transition to a coherently ordered BM phase.By comparing the
magnetic and electronic properties of the sample at
different oxygen deficientstates, we demonstrate that the
magnetic and electronic transitions are apart from the
structuralphase transition [1].Using in situ polarized
neutron reflectometry (PNR) measured at the MR reflectometer
(SNS/OakRidge), we explore the nuclear scattering density
(nSLD) and quantify the change in oxygen stoichiometryand
the magnetization of the LSCO film during annealing. The PNR
data shows a significantdecrease of nSLD for the annealed
film indicating a reduction in oxygen concentration. The
oxygenstoichiometry is found to vary from La0.6Sr0.4CoO3
before annealing to about La0.6Sr0.4CoO2.5for annealed
films. We find that disordered oxygen vacancies forming in
the initial phase of annealingquickly govern the magnetic
properties of the film by triggering a FM to AF transition
[1].[1] S. He, O. Petracic, V. Lauter, L. Cao, Y. Zhou, M.
L. Weber, J. Schubert, O. Concepción, R. Dittmann, R.
Waser, T. Brückel, F. Gunkel, La0.6Sr0.4CoO3−δ Films
Under Deoxygenation: Magnetic And Electronic Transitions Are
Apart from The Structural Phase TransitionAdv. Funct. Mater.
2024, 34, 2313208.},
month = {Oct},
date = {2024-10-08},
organization = {JCNS Workshop 2024, Trends and
Perspectives in Neutron Scattering:
Functional Interfaces, Evangelische
Akademie Tutzing (Germany), 8 Oct 2024
- 11 Oct 2024},
subtyp = {Invited},
cin = {JCNS-2 / JARA-FIT / PGI-7 / PGI-9},
cid = {I:(DE-Juel1)JCNS-2-20110106 / $I:(DE-82)080009_20140620$ /
I:(DE-Juel1)PGI-7-20110106 / I:(DE-Juel1)PGI-9-20110106},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G4 - Jülich Centre for Neutron
Research (JCNS) (FZJ) (POF4-6G4)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G4},
typ = {PUB:(DE-HGF)6},
url = {https://juser.fz-juelich.de/record/1031668},
}