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@ARTICLE{Vad:10331,
author = {Vad, T. and Sager, W. F. C. and Zhang, J. and Buitenhuis,
J. and Radulescu, A.},
title = {{E}xperimental determination of resolution function
parameters from small-angle neutron scattering data of a
colloidal {S}i{O}2 dispersion},
journal = {Journal of applied crystallography},
volume = {43},
issn = {0021-8898},
address = {Copenhagen},
publisher = {Munksgaard},
reportid = {PreJuSER-10331},
pages = {686 - 692},
year = {2010},
note = {The authors would like to thank Dr K. Nygard for assistance
in performing the SAXS experiments. Financial support by the
Bundesministerium fur Bildung und Forschung (BMBF), grant
No. 05 KS7OD2, is gratefully acknowledged.},
abstract = {A dilute dispersion of charge-stabilized, monodisperse
silica nanoparticles has been used to determine the
instrumental resolution function parameters of a
conventional small-angle neutron scattering instrument in
pinhole geometry over the entire accessible range of
momentum transfer q. Independent determination of the
structure parameters of the colloidal silica dispersion by
small-angle X-ray scattering enables refinement of both the
q-independent geometric and the q-dependent ( wavelength
spread or polychromaticity of the neutron beam)
contributions to the resolution function. The procedure
described is appropriate if no further instrumental
characterization is available. It is demonstrated that the
sample used for refining the resolution function parameters
has to exhibit sharp structural scattering features such as
Bragg reflections, form factor maxima and minima, or an
inter-particle correlation peak for each instrumental
configuration at which the measurements have been performed
to cover a q range of two orders of magnitude (0.03 < q <
3.2 nm(-1)).},
keywords = {J (WoSType)},
cin = {IFF-4 / IFF-5 / Jülich Centre for Neutron Science JCNS
(JCNS) ; JCNS / IFF-7},
ddc = {540},
cid = {I:(DE-Juel1)VDB784 / I:(DE-Juel1)VDB785 /
I:(DE-Juel1)JCNS-20121112 / I:(DE-Juel1)VDB787},
pnm = {BioSoft: Makromolekulare Systeme und biologische
Informationsverarbeitung (FUEK505) / Großgeräte für die
Forschung mit Photonen, Neutronen und Ionen (PNI) (FUEK415)
/ 450 - BioSoft (POF2-400)},
pid = {G:(DE-Juel1)FUEK505 / G:(DE-Juel1)FUEK415 /
G:(DE-HGF)POF2-450},
experiment = {EXP:(DE-MLZ)KWS2-20140101},
shelfmark = {Crystallography},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000279429500004},
doi = {10.1107/S0021889810022156},
url = {https://juser.fz-juelich.de/record/10331},
}