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@ARTICLE{Fischer:1033542,
author = {Fischer, Benedikt and Nuys, Maurice and Astakhov, Oleksandr
and Haas, Stefan and Schaaf, Michael and Besmehn, Astrid and
Jakes, Peter and Eichel, Rüdiger-A. and Rau, Uwe},
title = {{A}dvanced atmospheric pressure {CVD} of a-{S}i:{H} using
pure and cyclooctane-diluted trisilane as precursors},
journal = {Sustainable energy $\&$ fuels},
volume = {8},
number = {23},
issn = {2398-4902},
address = {Cambridge},
publisher = {Royal Society of Chemistry},
reportid = {FZJ-2024-06423},
pages = {5568 - 5580},
year = {2024},
abstract = {Liquid silanes can be used for low-cost, fast deposition of
hydrogenated amorphous silicon (a-Si:H) as an alternative to
state-of-the-art deposition processes such as plasma
enhanced chemical vapor deposition or electron beam
evaporation. However, liquid silane deposition techniques
are still in their infancy. In this paper, we present a new
version of the atmospheric pressure chemical vapor
deposition technique designed to improve the reproducibility
of a-Si:H deposition. With this new tool, we explore ways to
improve the quality of the material. The films can be
prepared using pure trisilane as a precursor; frequently,
however, trisilane is diluted with cyclooctane for better
handling and process control. Currently, the influence of
this dilution on the film quality is not well understood. In
our work, we investigate and compare both precursor
strategies. This paper presents a comprehensive analysis of
the effects of cyclooctane dilution, deposition temperature,
process duration, and precursor amount on the structure
stoichiometry and electronic properties of the resulting
films. The analysis was performed using a range of
techniques, including Fourier transform infrared
spectroscopy, electronic spin resonance spectroscopy, Raman
spectroscopy, ellipsometry, secondary ion mass spectrometry,
and conductivity measurements. For films deposited with pure
silane, we found a low oxygen (O) and carbon (C) impurity
incorporation and an adjustable H content up to $10\%,$
resulting in a photosensitivity of up to 104. Dependent on
the dilution and deposition temperature, the films deposited
with cyclooctane dilution showed various amounts of C
incorporation, culminating in an a-Si:H/a-SiC:H structure
for high temperatures and dilutions. High purity a-Si:H
films as a-Si:C:H films are promising for application in
solar cells and transistors either as an amorphous
functional layer or as a precursor for recrystallization
processes, e.g., in TOPCon solar cell technology.},
cin = {IMD-3 / ZEA-1 / IET-4 / IET-1},
ddc = {660},
cid = {I:(DE-Juel1)IMD-3-20101013 / I:(DE-Juel1)ZEA-1-20090406 /
I:(DE-Juel1)IET-4-20191129 / I:(DE-Juel1)IET-1-20110218},
pnm = {1212 - Materials and Interfaces (POF4-121) / 1223 -
Batteries in Application (POF4-122)},
pid = {G:(DE-HGF)POF4-1212 / G:(DE-HGF)POF4-1223},
typ = {PUB:(DE-HGF)16},
UT = {WOS:001344579800001},
doi = {10.1039/D4SE01308E},
url = {https://juser.fz-juelich.de/record/1033542},
}