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@ARTICLE{Szot:1033675,
author = {Szot, Krzysztof and Rodenbücher, Christian and Rogacki,
Krzysztof and Bihlmayer, Gustav and Speier, Wolfgang and
Roleder, Krystian and Krok, Franciszek and Keller, Hugo and
Simon, Arndt and Bussmann-Holder, Annette},
title = {{T}ransition to metallic and superconducting states induced
by thermalor electrical deoxidation of the dislocation
network in the surface regionof {S}r{T}i{O}3},
journal = {Nanomaterials},
volume = {14},
number = {23},
issn = {2079-4991},
address = {Basel},
publisher = {MDPI},
reportid = {FZJ-2024-06537},
pages = {1944 -},
year = {2024},
abstract = {The question as to why deoxidized SrTiO3−δ becomes
metallic and superconducting at extremely low levels of
oxygen vacancy concentration has been a mystery for many
decades. Here, we show that the real amount of effused
oxygen during thermal reduction, which is needed to induce
superconducting properties, is in the range of only 1014/cm3
and thus even lower than the critical carrier concentrations
assumed previously (1017–1019/cm3). By performing detailed
investigations of the optical and electrical properties down
to the nanoscale, we reveal that filaments are forming
during reduction along a network of dislocations in the
surface layer. Hence, a reduced epi-polished SrTiO3−δ
crystal has to be regarded as a nano-composite consisting of
a perfect dielectric matrix with negligible carrier density,
which is short-circuited by metallic filaments with a local
carrier density in the range of 1020/cm3. We present that
electro-degradation leads to a more pronounced evolution of
filamentary bundles and thus can generate a superconducting
state with higher TC than thermal reduction. These findings
indicate that traditional homogeneous models of
superconductivity in self-doped SrTiO3−δ need to be
revised, and we propose an alternative explanation taking
into account the coexistence of metallic dislocation cores
with polar insulating regions allowing for polaronic
coupling.},
cin = {IET-4 / PGI-1 / PGI-SO},
ddc = {540},
cid = {I:(DE-Juel1)IET-4-20191129 / I:(DE-Juel1)PGI-1-20110106 /
I:(DE-Juel1)PGI-SO-20200511},
pnm = {5211 - Topological Matter (POF4-521) / DFG project
G:(GEPRIS)491111487 - Open-Access-Publikationskosten / 2025
- 2027 / Forschungszentrum Jülich (OAPKFZJ) (491111487) /
1231 - Electrochemistry for Hydrogen (POF4-123)},
pid = {G:(DE-HGF)POF4-5211 / G:(GEPRIS)491111487 /
G:(DE-HGF)POF4-1231},
typ = {PUB:(DE-HGF)16},
pubmed = {39683332},
UT = {WOS:001376509400001},
doi = {10.3390/nano14231944},
url = {https://juser.fz-juelich.de/record/1033675},
}