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@INPROCEEDINGS{AzuaHumara:1034900,
author = {Azua Humara, Ana Daniela and Luna Barron, Ana Laura},
title = {{E}lectrocatalytic {A}mmonia {S}ynthesis {A}t {L}ow
{T}emperatures {A}nd {L}ow {P}ressures {I}n {A}queous
{M}edia},
school = {RWTH Aachen},
reportid = {FZJ-2025-00023},
year = {2024},
abstract = {Ammonia is one of the most produced chemical substances
globally and a key component in fertilizers. Its demand is
expected to rise significantly in the coming decades due to
population growth. However, the thermochemical Haber-Bosch
process, which is currently used to produce ammonia, is
highly energy-intensive and generates significant CO2
emissions. The international target is to reduce the ammonia
industry’s emissions to just 367 MtCO2 per year by 2050.
[1] Achieving this target requires decarbonizing ammonia
industry by implementing sustainable technologies. While
coupling the Harber-Bosch process with green hydrogen can
help reduce carbon emissions, projections indicate that
additional alternative technologies of ammonia production
will be necessary to meet the 2050 carbon target. [1] In
this context, electrochemical nitrogen reduction under
ambient conditions represents a promising approach to
complement the future technologies portfolio for green
ammonia production.Given the challenging and complex nature
of electrochemical nitrogen reduction, this PhD project
adopts a systematic research approach. The approach involves
separating the two key reaction steps—nitrogen activation
and nitrogen protonation—to study each in detail. This
will provide a deeper understanding that will guide the
design of an effective catalyst for ammonia production. The
first step, nitrogen activation, involves nitrogen
adsorption and the breaking of the highly stable nitrogen
triple bond. Because 941 kJ/mol of energy is required to
dissociate N₂ bonds, nitrogen activation is more difficult
than the nitrogen protonation step. Nitrogen protonation,
the second step, refers to the addition of protons (H⁺) to
nitrogen atoms to form ammonia (NH₃). Protonation is
closely related to the selectivity of the reaction, as
by-products like hydrazine can also form. Additionally,
protons may react to form hydrogen gas instead of ammonia,
which can further affect the reaction’s efficiency.This
progress report presents the results of the nitrogen
protonation investigation. The electrochemical nitrate
reduction reaction was selected as a model reaction because
it has lower energy requirements and shares key similarities
with nitrogen reduction reaction under ambient conditions.
These similarities include the competition with HER, the
formation of nitrogen-containing byproducts, and the
multistep proton-coupled electron transfers},
month = {Oct},
date = {2024-10-28},
organization = {IET-1 PhD Autumn Seminar, Düren
(Germany), 28 Oct 2024 - 30 Oct 2024},
subtyp = {Other},
cin = {IET-1},
cid = {I:(DE-Juel1)IET-1-20110218},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123) / BMBF
03SF0589B - Verbundvorhaben iNEW: Inkubator Nachhaltige
Elektrochemische Wertschöpfungsketten (iNEW) im Rahmen des
Gesamtvorhabens Accelerator Nachhaltige Bereitstellung
Elektrochemisch Erzeugter Kraft- und Wertstoffe mittels
Power-to-X (ANABEL) (03SF0589B) / HITEC - Helmholtz
Interdisciplinary Doctoral Training in Energy and Climate
Research (HITEC) (HITEC-20170406)},
pid = {G:(DE-HGF)POF4-1231 / G:(BMBF)03SF0589B /
G:(DE-Juel1)HITEC-20170406},
typ = {PUB:(DE-HGF)31},
url = {https://juser.fz-juelich.de/record/1034900},
}