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@ARTICLE{Thienenkamp:1035293,
author = {Thienenkamp, Johannes H. and Lennartz, Peter and Winter,
Martin and Brunklaus, Gunther},
title = {{E}xperimental correlation of anionic mass transport and
lithium dendrite growth in solid-state polymer-based lithium
metal batteries},
journal = {Cell reports / Physical science},
volume = {5},
number = {12},
issn = {2666-3864},
address = {[New York, NY]},
publisher = {Elsevier},
reportid = {FZJ-2025-00351},
pages = {102340 - 102352},
year = {2024},
abstract = {Various metal deposition models have been proposed for
alkali metal batteries, but the experimental acces-sibility
of designated driving forces and characteristics of specific
morphologies is still limited. A combinedmethod portfolio
comprising operando 1D 19 F MRI, in situ 7 Li NMR, and
dynamic electrochemical impedancespectroscopy (EIS)
experiments is presented. Experimental evidence of the
relation of capacity-degradingdendritic Li metal growth and
anionic mass-transport quantities beyond Sand’s time in
polymer-based Limetal batteries is demonstrated. Comparison
of anionic mass transport and morphological changes in
Limetal in Li||Li and NMC 622||Li cells revealed that
elevated anion drift velocities within electrolytes are
corre-lated with pronounced dendrite growth. Higher cell
voltages are associated with increased anion drift
veloc-ities and hence dendrite growth, as reflected by a
2.5-fold increase in velocities in NMC 622||Li compared to
Li||Li cells. This highlights the potential of the
introduced method portfolio for experimental evaluation of
poly-mer electrolytes and artificial coatings suitable for
alkali metal batteries},
cin = {IMD-4},
ddc = {530},
cid = {I:(DE-Juel1)IMD-4-20141217},
pnm = {1222 - Components and Cells (POF4-122) / For-Analytik
(BMBF-13XP0445) / FB2-POLY - Zellplattform Polymere
(BMBF-13XP0429A)},
pid = {G:(DE-HGF)POF4-1222 / G:(DE-Juel1)BMBF-13XP0445 /
G:(DE-Juel1)BMBF-13XP0429A},
typ = {PUB:(DE-HGF)16},
UT = {WOS:001391642100001},
doi = {10.1016/j.xcrp.2024.102340},
url = {https://juser.fz-juelich.de/record/1035293},
}