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@INPROCEEDINGS{Bostrm:1037739,
author = {Boström, Oskar and Choi, Seung-Young and Xia, Lu and
Lohmann-Richters, Felix and Jannasch, Patric},
title = {({P}oster {A}ward - {H}onorable {M}ention) {D}urable
{P}olybenzimidazole {A}nion {E}xchange {M}embranes for
{A}lkaline {W}ater {E}lectrolyzers},
issn = {2151-2043},
reportid = {FZJ-2025-00899},
year = {2023},
abstract = {Water electrolysis under alkaline conditions allows the use
of inexpensive non-platinum-group catalysts such as
nickel.1, 2 Conventional alkaline electrolyzers usually
employ a highly concentrated aq. KOH solution as electrolyte
(5-7 M) with a porous diaphragm as separator. Alternatively,
protolysable polymers such as polybenzimidazole (PBI) may be
swollen with electrolyte and used as ion-solvating
membranes.2, 3 However, the chemical stability of the
polymers can become a serious issue under these harsh
conditions. Operation under more dilute conditions, e.g., up
to 2 M KOH, may bring the benefits of the alkaline
conditions combined with a longer cell lifetime. Under these
conditions, aliphatic cyclic quaternary ammonium (QA)
cations, such as piperidinium, have shown excellent
stability.In the present work, performed as part of the EU
project "NEXTAEC", we have designed and synthesized m-PBI
grafted with mono- and bis-piperidinium functionalized side
chains, respectively (Figure 1a-b). AEMs were prepared from
polymers with varying ion exchange capacities and studied at
80 °C containing KOH solutions in the concentration range
0.5-2 M KOH. The membranes were characterized with respect
to, e.g., electrolyte solution uptake, alkaline stability,
and electrolyser performance (Figure 1c). The uptake showed
a strong inverse correlation with KOH concentration, which
also affected the electrochemical performance. The stability
as evaluated by 1HNMR spectroscopy was excellent showing, in
the worst case, less than 8 $\%$ ionic loss after 6 months
storage in 2 M KOH at 80 °C.},
month = {Oct},
date = {2023-10-08},
organization = {244th ECS Meeting, Gothenburg
(Sweden), 8 Oct 2023 - 12 Oct 2023},
cin = {IEK-14 / IET-4},
ddc = {540},
cid = {I:(DE-Juel1)IEK-14-20191129 / I:(DE-Juel1)IET-4-20191129},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123)},
pid = {G:(DE-HGF)POF4-1231},
typ = {PUB:(DE-HGF)1},
doi = {10.1149/MA2023-02391889mtgabs},
url = {https://juser.fz-juelich.de/record/1037739},
}