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@ARTICLE{Stroyuk:1044610,
author = {Stroyuk, Oleksandr and Raievska, Oleksandra and Kinge,
Sachin and Hauch, Jens and Brabec, Christoph},
title = {{E}xploring compositional versatility of perovskite-like
{C}s 3 ({B}i,{S}b) 2 {X} 9 ({X} = {C}l, {B}r, {I}) compounds
by high-throughput experimentation},
journal = {Materials advances},
volume = {6},
number = {14},
issn = {2633-5409},
address = {Cambridge},
publisher = {Royal Society of Chemistry},
reportid = {FZJ-2025-03281},
pages = {4847 - 4856},
year = {2025},
abstract = {A high-throughput compositional screening of
perovskite-like Cs3M2X9 double salts (M = Bi and Sb and X =
Cl, Br, and I) allows independent variation of the M and X
components, yielding one hundred single-phase products
within a general synthetic approach that combines engineered
precipitation of chloride and bromide precursors and their
anion exchange conversion into more complex halide
derivatives. The X variation at a fixed M = Bi3+ yields
various single-phase Cs3Bi2X9 compounds with X = Cl, Cl +
Br, Br, Br + I, and Cl + Br + I. The anion exchange in
chlorides with Br + I combinations produces stable Cs3Bi2X9
compounds with all three halides simultaneously present in
the lattice, and Cl, Br, and I contents varied in the ranges
of ca. $40–90\%,$ $10–60\%,$ and $30–90\%,$
respectively. The presence of bromide, even as a residue,
enables the co-existence of Cl and I, and dictates the
trigonal symmetry, in contrast to the hexagonal symmetry
typical for Cs3M2I9. The compounds with X = Cl + Br + I show
band gap variations in the range of 2.0–2.5 eV and linear
dependencies on the iodide content and lattice parameters.
The simultaneous variation of the X and M sites yields
single-phase Cs3(Bi,Sb)2X9 solid-solution compounds with
tailorable X and a Bi/Sb ratio varied from 0 to 1.0. All
Bi/Sb families reveal a band bowing effect, with the band
gaps of mixed Bi/Sb compounds being lower than those of Bi-
and Sb-only counterparts. The bowing parameter depends on
the X subsystem, decreasing from 0.80 eV for Cl to 0.60 eV
for Cl + Br and 0.40–0.45 eV for Br and Br + I, indicating
that chemical variations in the mixed Bi/Sb lattices, rather
than local disorders or lattice strains, govern the
band-bowing behavior.},
cin = {IET-2},
ddc = {540},
cid = {I:(DE-Juel1)IET-2-20140314},
pnm = {1213 - Cell Design and Development (POF4-121)},
pid = {G:(DE-HGF)POF4-1213},
typ = {PUB:(DE-HGF)16},
UT = {WOS:001510666400001},
doi = {10.1039/D5MA00479A},
url = {https://juser.fz-juelich.de/record/1044610},
}