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@INPROCEEDINGS{Zeng:1046967,
author = {Zeng, Yuan and Leonard, Kwati and Guillon, Olivier and
Menzler, Norbert H.},
title = {{F}abrication of {T}hin {E}lectrolyte via {W}et {P}owder
{S}praying and {I}nvestigation of {I}ts {S}intering
{B}ehavior for {S}olid {O}xide {P}roton {C}onducting
{C}ells},
reportid = {FZJ-2025-04035},
year = {2025},
abstract = {Solid state proton conducting fuel and electrolysis cells
have attracted significant attention due to their potential
to operate at relatively low temperatures (400–600°C).
Electrolytes with reduced thickness can decrease ohmic
resistance, enabling enhanced cell performance under the
sluggish kinetics typical at low temperatures. Among the
ceramic thin-film deposition methods that are easy to
process and suitable for scale-up, such as tape casting and
screen printing, the capability of wet powder spraying for
preparing thin electrolytes has been largely underestimated.
Here, we developed a wet powder spraying process that
eliminates the need for additional organic additives such as
binders and dispersants in the suspension. The electrolytes
with thickness below 5 μm were we successfully fabricated
through parameter optimization.Besides, acceptor-doped
Ba(Zr, Ce)O₃ proton conductors has long suffered from
sintering challenges. Sintering at high temperature is
unavoidable due to the high refractory nature of its
constituent elements. However, Ba tends to evaporate at
elevated temperatures (above 1400°C), degrading
conductivity and cause B-site elements segregation. This
Ba-evaporation issue becomes particularly severe during
co-sintering of half-cells with thin electrolytes. We
propose two solutions: (1) optimizing substrate and
electrolyte compositions to lower the co-sintering
temperature; (2) employing a simple Ba compensation strategy
to counteract evaporation and improve sintering. Overall,
the combination of the wet powder spraying process and
sintering optimization enables the fabrication of thin,
dense electrolyte. The resulting full cells exhibit
promising electrochemical performance.},
month = {Aug},
date = {2025-08-31},
organization = {The XIXth ECerS Conference 2025,
Dresden (Germany), 31 Aug 2025 - 4 Sep
2025},
subtyp = {Other},
cin = {IMD-2},
cid = {I:(DE-Juel1)IMD-2-20101013},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123) / SOFC -
Solid Oxide Fuel Cell (SOFC-20140602)},
pid = {G:(DE-HGF)POF4-1231 / G:(DE-Juel1)SOFC-20140602},
typ = {PUB:(DE-HGF)6},
url = {https://juser.fz-juelich.de/record/1046967},
}