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@ARTICLE{Morsa:1047173,
author = {Morsa, Amedeo and Yazhenskikh, Elena and Jacob, Rhys
Dominic and Müller, Michael and Sergeev, Dmitry},
title = {{T}hermodynamics of the {M}g{C}l2-{M}g{SO}4 and
{C}a{C}l2-{C}a{SO}4 systems},
journal = {Calphad},
volume = {91},
issn = {0364-5916},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2025-04130},
pages = {102888},
year = {2025},
abstract = {Thermodynamic properties of MgCl2-MgSO4 and CaCl2-CaSO4
binary systems hold significant importance in the
exploration of potential phase change materials for thermal
energy storage applications. This study aims to elucidate
the phase diagrams and thermodynamic properties of the
eutectic mixtures within these systems, employing
experimental techniques such as Differential Thermal
Analysis (DTA) and Differential Scanning Calorimetry (DSC).
Through comprehensive experimental investigations, the phase
diagrams of the MgCl2-MgSO4 and CaCl2-CaSO4 systems were
meticulously delineated, revealing the eutectic compositions
and transition temperatures. Specifically, the eutectic
composition for MgCl2-MgSO4 was proposed to be 28.0 $mol\%$
MgSO4 with a melting temperature of 663 ± 5 °C, while for
the CaCl2-CaSO4 system it was found to be at 14.0 $mol\%$
CaSO4 and 722 ± 5 °C. Additionally, the enthalpy of fusion
of these eutectic mixtures was for the first time
determined, providing crucial insights into their thermal
behaviour. They are 38.2 ± 1.0 kJ/mol for the Mg-containing
system and 30.2 ± 0.4 kJ/mol for the Ca-containing system,
respectively. The experimental data obtained in this study
served as the foundation for the development of a new Gibbs
energy dataset, which is essential for conducting
thermodynamic calculations. The utilisation of this dataset
enables accurate predictions of thermodynamic properties
across the entire composition and temperature ranges of the
systems under investigation.},
cin = {IMD-1},
ddc = {540},
cid = {I:(DE-Juel1)IMD-1-20101013},
pnm = {1243 - Thermal Energy Storage (POF4-124) / BMWK 01GW0623 -
Verbundvorhaben: PCM-Screening-2 - Evaluierung von
Salzsystemen für den Einsatz als PCM: thermodynamische
Modellierung und experimentelle Methoden - 2; Teilvorhaben:
Thermochemie wasserfreier Salzsysteme für PCM (01GW0623)},
pid = {G:(DE-HGF)POF4-1243 / G:(BMWK)01GW0623},
typ = {PUB:(DE-HGF)16},
doi = {10.1016/j.calphad.2025.102888},
url = {https://juser.fz-juelich.de/record/1047173},
}