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@PHDTHESIS{Hamacher:1047702,
author = {Hamacher, Stefanie},
title = {{D}evelopment of a {N}ew, {M}iniaturized and {F}lexible
{T}emperature {S}ensor},
volume = {303},
school = {RWTH Aachen University},
type = {Dissertation},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2025-04468},
isbn = {978-3-95806-863-6},
series = {Schriften des Forschungszentrums Jülich Reihe
Schlüsseltechnologien / Key Technologies},
pages = {XXII, 153},
year = {2025},
note = {Dissertation, RWTH Aachen University, 2025},
abstract = {Temperature is one of the most important scientific
quantities and plays a fundamental part in our daily life.
While permanent temperature sensors were primarily used to
control air conditioning, fridges and freezers, nowadays
they are utilized in many more fields, such as healthcare,
manufacturing and agriculture. Over the centuries several
different devices were developed that were able to determine
changes in temperature. In the beginning, such a thermometer
was simply based on the expansion and contraction of air or
water and the dilation of liquids is still in use in the
common mercury thermometer. However, many more devices are
known today that are based on the change of different
physical quantities that can be related to temperature.
Common examples are the change in resistance used in
resistance temperature detectors (RTDs) or thermistors or
the change in spectral characteristics detected via IR
measurements. Depending on the purpose of the temperature
measurement an appropriate technique is chosen, since all of
the known devices have their advantages and drawbacks, e.g.
a small temperature range or low relative change of the
specific parameter per degree. To overcome such drawbacks, a
miniaturized temperature sensor based on a new approach was
developed in this work. As a sensing principle, the
dependence of the diffusion coefficient on fluid viscosity,
which in turn is temperature dependent, was exploited. Using
Faradaic electrochemical currents from a redox mediator
dissolved in fluid, a relation between current and
temperature can be obtained. Here, three different ionic
liquids (ILs) and mixtures of them were investigated along
with different redox species, such as ferrocene,
hydroquinone and methylene blue to establish a stable
temperature sensor that is suitable over a large temperature
range and shows long-term stability. Several thin-film
sensor prototypes were fabricated and characterized using
custom-made electronics as well as a potentiostat. First,
the peak current dependence on temperature using cyclic
voltammetry (CV) was demonstrated. Afterwards a screening of
the most feasible redox species was conducted using CV.
Thereby it was found that ferrocene is not stable over a
longer period of time, which is why other redox couples were
examined and methylene blue was found to be the best.
Additionally, the IL 1-ethylimidazolium nitrate ([EIM][NO3])
was used as redox species and solvent medium simultaneously.
In order to establish an easy to handle sensor, the
sensitive layer had to be fixed upon the substrate. This was
achieved by adding two monomers and a photo initiator to the
IL mixture that were cured using UV light. Finally, the
prepared temperature sensors were characterized using the
chronoamperometric technique and four different pulse
lengths. Compared to standard resistance temperature
detectors, this novel sensor shows a higher per degree
sensitivity and can be utilized in a broad temperature
range, for example for cold-chain monitoring of
perishables.},
cin = {IBI-3},
cid = {I:(DE-Juel1)IBI-3-20200312},
pnm = {899 - ohne Topic (POF4-899)},
pid = {G:(DE-HGF)POF4-899},
typ = {PUB:(DE-HGF)3 / PUB:(DE-HGF)11},
urn = {urn:nbn:de:0001-2602091348143.817852468181},
doi = {10.34734/FZJ-2025-04468},
url = {https://juser.fz-juelich.de/record/1047702},
}