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@ARTICLE{Haneke:1048484,
author = {Haneke, Lukas and Pfeiffer, Felix and Rudolf, Katharina and
Sutar, Pranti and Baghernejad, Masoud and Winter, Martin and
Placke, Tobias and Kasnatscheew, Johannes},
title = {{I}nvestigating the {E}xistence of a {C}athode
{E}lectrolyte {I}nterphase on {G}raphite in {D}ual‐{I}on
{B}atteries with {L}i{PF} 6 ‐{B}ased {A}protic
{E}lectrolytes and {U}nraveling the {O}rigin of {C}apacity
{F}ade},
journal = {Advanced energy $\&$ sustainability research},
volume = {6},
number = {3},
issn = {2699-9412},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2025-04673},
pages = {2400330},
year = {2025},
abstract = {This study elucidates the presence of a cathode electrolyte
interphase (CEI) at graphite positive electrodes (PEs) and
assesses its impact on the performance of dual-ion
batteries, being promising candidates for cost-efficient and
sustainable stationary energy storage. Indeed, electrolyte
oxidation increases during charge (5 V vs Li|Li+) for
decreased C rates, that is longer duration at high
state-of-charges (SOC) , but effective protection and
evidence for CEI formation is missing as no increase in
Coulombic efficiencies is observed, even with
literature-known electrolyte additives like vinylene
carbonate, fluoroethylene carbonate, or ethylene sulfite in
a highly concentrated base electrolyte (4.0 m LiPF6 in
dimethyl carbonate) as reference. Via studying charged and
pristine PEs by X-ray photoelectron spectroscopy,
PF6−-graphite intercalation compounds and cointercalated
solvent molecules are identified, while indications for CEI
are absent within 1000 charge/discharge cycles.
Nevertheless, a high capacity retention of $≈94\%$
(referring to 0.1C) is demonstrated. Affirmed by Raman
spectroscopy and scanning electron microscopy, the active
material remains structurally stable, suggesting capacity
fading to be dominated by resistance rise at the PE, likely
due to an electronic contact resistance from active material
grain boundaries and/or from the interface between electrode
particles and the current collector in course of high volume
changes; as systematically derived by impedance
spectroscopy.},
cin = {IMD-4},
ddc = {333.7},
cid = {I:(DE-Juel1)IMD-4-20141217},
pnm = {1223 - Batteries in Application (POF4-122)},
pid = {G:(DE-HGF)POF4-1223},
typ = {PUB:(DE-HGF)16},
UT = {WOS:001373740100001},
doi = {10.1002/aesr.202400330},
url = {https://juser.fz-juelich.de/record/1048484},
}