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@ARTICLE{Mielke:1050634,
author = {Mielke, Kristina and Ickenroth, Philipp and Jupke, Andreas},
title = {{E}xperimental {S}etup for {U}nderstanding the {I}nfluence
of {W}all {C}ontact of {S}tructured {P}acking {M}aterial on
{D}rop {S}edimentation in {L}iquid–{L}iquid {S}ystems},
journal = {Industrial $\&$ engineering chemistry research},
volume = {64},
number = {36},
issn = {0888-5885},
address = {Columbus, Ohio},
publisher = {American Chemical Society},
reportid = {FZJ-2026-00386},
pages = {17685 - 17695},
year = {2025},
note = {Grant: Exploratory Research Space: Seed Fund (2) als
Anschubfinanzierung zur Erforschung neuer
interdisziplinärer Ideen (RWTH intern)},
abstract = {To model liquid–liquid extraction columns (LLE-columns)
accurately, correlations for occurring phenomena inside the
columns (e.g., drop sedimentation) are necessary. Currently,
existing correlations for the sedimentation velocity of
drops in LLE-columns equipped with structured packings do
not consider the interaction of the drops with different
packing material surfaces or the complex geometry of those.
Therefore, utilizing these correlations for designing these
LLE-columns still exhibits high uncertainties, which
commonly necessitate cost- and time-expensive experiments.
To accelerate the efficiency of the design of these
LLE-columns, we present a measuring cell in which single
drop-wall interactions can be investigated. To quantify the
drop-wall interaction, drop velocity, contact angle, and
contact line can be measured optically while varying the
counter-current flow, drop size, tilting angle, and surface
material. The experimentally determined velocities are in
accordance with sedimentation velocities in structured
packings. Common correlations for sedimentation velocities
in structured packings turned out not to be universally
applicable.},
cin = {IBG-2},
ddc = {660},
cid = {I:(DE-Juel1)IBG-2-20101118},
pnm = {2172 - Utilization of renewable carbon and energy sources
and engineering of ecosystem functions (POF4-217)},
pid = {G:(DE-HGF)POF4-2172},
typ = {PUB:(DE-HGF)16},
doi = {10.1021/acs.iecr.5c01952},
url = {https://juser.fz-juelich.de/record/1050634},
}