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@ARTICLE{Zheng:1050783,
author = {Zheng, Hongkui and Chakraborty, Pritam K and Spruit, Ronald
and Pivak, Yevheniy and Sun, Hongyu and Basak, Shibabrata
and Eichel, Rüdiger-A and Garza, Hugo Pérez},
title = {{M}odulating {M}etal {S}upport {I}nteractions for {D}urable
and {S}elective {CO}2 {H}ydrogenation {R}eaction: {A}n
{O}perando {T}ransmission {E}lectron {M}icroscopy {S}tudy},
journal = {Microscopy and microanalysis},
volume = {31},
number = {$Supplement_1$},
issn = {1079-8501},
address = {Oxford},
publisher = {Oxford University Press},
reportid = {FZJ-2026-00507},
pages = {ozaf048.923},
year = {2025},
abstract = {Carbon dioxide (CO2) hydrogenation is a promising route to
generate clean high-value fuels and chemicals, for example
CO, CH4, CH3OH, and C2+ hydrocarbons. Heterogeneous
metal-support catalysts have emerged as prime candidates for
this reaction, effectively dissociating H2 to facilitate CO2
conversion. While considerable effort has focused on
tailoring the size, morphology, and composition of both
supports and metal nanoparticles, achieving high activity,
selectivity, and stability remains a significant challenge.
Crucially, metal-support interactions (MSI) are now
recognized as playing a decisive role, as the interface
provides active sites and oxygen vacancies that influence
gas adsorption, activation, and product formation.
Therefore, directly observing these dynamic MSI under
realistic reaction conditions is essential for understanding
catalytic mechanisms and designing advanced catalysts.While
various in-situ techniques have been employed to probe CO2
hydrogenation, recent advances in MEMS-based sample carriers
and corresponding transmission electron microscopy (TEM)
holders, coupled with residual gas analysis, have enabled
in-situ TEM studies of near-atmospheric pressure reactions.
As TEM provides the opportunity to perform simultaneous
high-resolution imaging, chemical composition mapping, and
local electronic structure studies, in-situ TEM allows for
real-time observation of MSI dynamics and correlation with
reaction products, providing unprecedented insights into the
catalytic processes.In this work, by comparing different
types of metal-substrate interaction, we will uncouple the
effect of substrate during CO2 hydrogenation. Our study
would contribute to deepening the understanding of high
temperature (co)electrolysis processes, leading to the
design of high-performance electrode materials.},
cin = {IET-1},
ddc = {500},
cid = {I:(DE-Juel1)IET-1-20110218},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123) / HITEC -
Helmholtz Interdisciplinary Doctoral Training in Energy and
Climate Research (HITEC) (HITEC-20170406)},
pid = {G:(DE-HGF)POF4-1231 / G:(DE-Juel1)HITEC-20170406},
typ = {PUB:(DE-HGF)16},
doi = {10.1093/mam/ozaf048.923},
url = {https://juser.fz-juelich.de/record/1050783},
}