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@ARTICLE{vonWestarp:1052065,
author = {von Westarp, William Graf and Hense, Janik and Haas, Moritz
and Jupke, Andreas},
title = {{T}erpenoids as solvents for the separation of
2,3-butanediol from water: {P}hase equilibria and process
evaluation},
journal = {Fluid phase equilibria},
volume = {600},
issn = {0378-3812},
address = {New York, NY [u.a.]},
publisher = {Science Direct},
reportid = {FZJ-2026-00735},
pages = {114572 -},
year = {2026},
abstract = {2,3-butanediol (2,3-BDO) is a versatile platform chemical
that can be produced via fermentation in aqueous solution.
The energy intensive recovery of the high boiling 2,3-BDO
from water via distillation hinders the economic viability
of biotechnological produced 2,3-BDO. Hence,
extraction-distillation processes using novel solvents from
the class of terpenoids, namely menthol, thymol, and
carvacrol, are proposed. To this end, binary and ternary
liquid-liquid equilibrium (LLE) data for H2O, 2,3-BDO, and
each terpenoid, as well as boiling point data for 2,3-BDO
and the respective terpenoid, are measured. The
thermodynamic phase equilibria are correlated with the
non-random two liquid (NRTL) model and consecutive process
design of the extraction-distillation processes is conducted
using Aspen Plus. Conventional solvents (isobutanol,
1-butanol, and oleylalcohol), thymol, and carvacrol are
assessed in terms of specific exergy demand for the
production of 2,3-BDO. The lowest specific exergy demands
were found for oleyl alcohol (5.38 kJ g−1) and thymol
(5.14 kJ g−1), carvacrol (5.49 kJ g−1). Hence,
terpenoids are a competitive class of solvents and should be
included in solvent screening approaches.},
cin = {IBG-2},
ddc = {540},
cid = {I:(DE-Juel1)IBG-2-20101118},
pnm = {2172 - Utilization of renewable carbon and energy sources
and engineering of ecosystem functions (POF4-217) / PFExC006
- EXC2186 "The Fuel Science Center" (EXS-PF-PFExC006) /
BioSC - Bioeconomy Science Center (BioSC)},
pid = {G:(DE-HGF)POF4-2172 / G:(DE-82)EXS-PF-PFExC006 /
G:(DE-Juel1)BioSC},
typ = {PUB:(DE-HGF)16},
doi = {10.1016/j.fluid.2025.114572},
url = {https://juser.fz-juelich.de/record/1052065},
}