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001055036 0247_ $$2datacite_doi$$a10.34734/FZJ-2026-01833
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001055036 041__ $$aEnglish
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001055036 1001_ $$0P:(DE-Juel1)190603$$aHilger, Martin$$b0
001055036 1112_ $$a19th International Symposium on Solid Oxide Fuel Cells$$cStockholm$$gSOFC-XIX$$wSweden
001055036 245__ $$aElectrophoretic Deposition of Protective Spinel Coatings for Solid Oxide Cell Interconnects – Towards Stack Integration
001055036 260__ $$aBristol$$bIOP Publishing$$c2026
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001055036 520__ $$aWe evaluated electrophoretic deposition (EPD) of spinel coatings for solid oxide cell (SOC) interconnects with a focus on stack integration. Two compositions, MnCo1.9Fe0.1O4 (MCF) and CuMn1.8Ni0.2O4 (CMN), were deposited from water/ethanol suspensions and subjected to three thermal routes: direct oxidation and two-step treatments with reduction in Ar/H2 at 900 or 1000 °C followed by oxidation. Structural evolution, chromium evaporation, mass gain, and ex situ area-specific resistance (ASR) were assessed. Sealant compatibility with a Ca-Ba-silicate glass and applicability to representative flow-field geometries were investigated. All coatings formed continuous layers; two-step treatments enhanced densification compared to direct oxidation. Prereduction of MCF layers at 1000 °C yielded the lowest Cr evaporation and mass gain, whereas CMN exhibited chromium ingress, phase variations, and coarsened microstructures. ASR values for all types remained around or below 20 mΩ cm2. Glass-joining produced dense composites; limited cation diffusion was observed for MCF, while CMN showed substantial Cu penetration into the glass. EPD produced uniform, defect-free coatings on complex flow-field structures, with only slight thickness variations across the profile. These results support MCF-EPD with a 1000 °C reduction step and in situ oxidation during stack assembly as a process-compatible route for protective interconnect coatings in high-temperature SOCs, while CMN remains of particular interest for intermediate-temperature applications.
001055036 536__ $$0G:(DE-HGF)POF4-1231$$a1231 - Electrochemistry for Hydrogen (POF4-123)$$cPOF4-123$$fPOF IV$$x0
001055036 536__ $$0G:(EU-Grant)101058784$$aNOUVEAU - NOVEL ELECTRODE COATINGS AND INTERCONNECT FOR SUSTAINABLE AND REUSABLE SOEC (101058784)$$c101058784$$fHORIZON-CL4-2021-RESILIENCE-01$$x1
001055036 536__ $$0G:(DE-Juel1)SOFC-20140602$$aSOFC - Solid Oxide Fuel Cell (SOFC-20140602)$$cSOFC-20140602$$fSOFC$$x2
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001055036 7001_ $$0P:(DE-HGF)0$$aKrogsgaard, Thorbjørn$$b1
001055036 7001_ $$0P:(DE-Juel1)133667$$aGroß-Barsnick, Sonja-Michaela$$b2
001055036 7001_ $$0P:(DE-Juel1)129662$$aSebold, Doris$$b3
001055036 7001_ $$0P:(DE-HGF)0$$aShrikanth, S.$$b4
001055036 7001_ $$0P:(DE-HGF)0$$aFroitzheim, Jan$$b5
001055036 7001_ $$0P:(DE-Juel1)138081$$aLenser, Christian$$b6$$eCorresponding author
001055036 7001_ $$0P:(DE-Juel1)129636$$aMenzler, Norbert H.$$b7$$eCorresponding author
001055036 770__ $$aFocus Issue on SOFC XIX: Advances in Solid Oxide Fuel Cell and Electrolysis Cell Technology
001055036 773__ $$0PERI:(DE-600)2002179-3$$a10.1149/1945-7111/ae3ebb$$gVol. 173, no. 3, p. 034509 -$$n3$$p034509$$tJournal of the Electrochemical Society$$v173$$x0013-4651$$y2026
001055036 8564_ $$uhttps://juser.fz-juelich.de/record/1055036/files/Hilger_2026_J._Electrochem._Soc._173_034509.pdf$$yOpenAccess
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