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@ARTICLE{Wang:111912,
author = {Wang, Z. and Schröder, G.F.},
title = {{R}eal-space {R}efinement with {D}ire{X}: {F}rom {G}lobal
{F}itting to {S}ide-chain {I}mprovements},
journal = {Biopolymers},
volume = {97},
issn = {0006-3525},
address = {New York, NY},
publisher = {Wiley},
reportid = {PreJuSER-111912},
pages = {S687 - S697},
year = {2012},
note = {Record converted from VDB: 16.11.2012},
abstract = {Single-particle cryo-electron microscopy (cryo-EM) has
become an important tool to determine the structure of large
biomolecules and assemblies thereof. However, the achievable
resolution varies considerably over a wide range of about
3.5-20 Å. The interpretation of these intermediate- to
low-resolution density maps in terms of atomic models is a
big challenge and an area of active research. Here, we
present our real-space structure refinement program DireX,
which was developed primarily for cryo-EM-derived density
maps. The basic principle and its main features are
described. DireX employs Deformable Elastic Network (DEN)
restraints to reduce overfitting by decreasing the effective
number of degrees of freedom used in the refinement. Missing
or reduced density due to flexible parts of the protein can
lead to artifacts in the structure refinement, which is
addressed through the concept of restrained grouped
occupancy refinement. Furthermore, we describe the
performance of DireX in the 2010 Cryo-EM Modeling Challenge,
where we chose six density maps of four different proteins
provided by the Modeling Challenge exemplifying typical
refinement results at a large resolution range from 3 to 23
Å.},
keywords = {Antigens, Viral: chemistry / Aquaporins: chemistry / Capsid
Proteins: chemistry / Chaperonin 10: chemistry / Chaperonin
60: chemistry / Cryoelectron Microscopy: methods / Eye
Proteins: chemistry / Models, Molecular / Proteins:
chemistry / Software / Antigens, Viral (NLM Chemicals) /
Aquaporins (NLM Chemicals) / Capsid Proteins (NLM Chemicals)
/ Chaperonin 10 (NLM Chemicals) / Chaperonin 60 (NLM
Chemicals) / Eye Proteins (NLM Chemicals) / Proteins (NLM
Chemicals) / VP6 protein, Rotavirus (NLM Chemicals) /
aquaporin 0 (NLM Chemicals) / J (WoSType)},
cin = {ICS-6},
ddc = {570},
cid = {I:(DE-Juel1)ICS-6-20110106},
pnm = {Funktion und Dysfunktion des Nervensystems / BioSoft:
Makromolekulare Systeme und biologische
Informationsverarbeitung},
pid = {G:(DE-Juel1)FUEK409 / G:(DE-Juel1)FUEK505},
shelfmark = {Biochemistry $\&$ Molecular Biology / Biophysics},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:22696405},
UT = {WOS:000305183000005},
doi = {10.1002/bip.22046},
url = {https://juser.fz-juelich.de/record/111912},
}