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@ARTICLE{Finck:111944,
author = {Finck, N. and Dardenne, K. and Bosbach, D. and Geckeis, H.},
title = {{S}elenide {R}etention by {M}ackinawite},
journal = {Environmental science $\&$ technology},
volume = {46},
issn = {0013-936X},
address = {Columbus, Ohio},
publisher = {American Chemical Society},
reportid = {PreJuSER-111944},
pages = {10004 - 10011},
year = {2012},
note = {Record converted from VDB: 16.11.2012},
abstract = {The isotope (79)Se may be of great concern with regard to
the safe disposal of nuclear wastes in deep geological
repositories due to its long half-life and potential
mobility in the geosphere. The Se mobility is controlled by
the oxidation state: the oxidized species (Se(IV)) and
(Se(VI)) are highly mobile, whereas the reduced species
(Se(0) and Se(-II)) form low soluble solids. The mobility of
this trace pollutant can be greatly reduced by interacting
with the various barriers of the repository. Numerous
studies report on the oxidized species retention by mineral
phases, but only very scarce studies report on the selenide
(Se(-II)) retention. In the present study, the selenide
retention by coprecipitation with and by adsorption on
mackinawite (FeS) was investigated. XRD and SEM analyses of
the samples reveal no significant influence of Se on the
mackinawite precipitate morphology and structure. Samples
from coprecipitation and from adsorption are characterized
at the molecular scale by a multi-edge X-ray absorption
spectroscopy (XAS) investigation. In the coprecipitation
experiment, all elements (S, Fe, and Se) are in a low ionic
oxidation state and the EXAFS data strongly point to
selenium located in a mackinawite-like sulfide environment.
By contacting selenide ions with FeS in suspension, part of
Se is located in an environment similar to that found in the
coprecipitation experiment. The explanation is a dynamical
dissolution-recrystallization mechanism of the highly
reactive mackinawite. This is the first experimental study
to report on selenide incorporation in iron monosulfide by a
multi-edge XAS approach.},
cin = {IEK-6},
ddc = {050},
cid = {I:(DE-Juel1)IEK-6-20101013},
pnm = {Nukleare Sicherheitsforschung},
pid = {G:(DE-Juel1)FUEK404},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:22900520},
UT = {WOS:000308787800024},
doi = {10.1021/es301878y},
url = {https://juser.fz-juelich.de/record/111944},
}