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@ARTICLE{Kubicek:111979,
author = {Kubicek, J. and Schlesinger, R. and Baeken, C. and Büldt,
G. and Schäfer, F. and Labahn, J.},
title = {{C}ontrolled {I}n {M}eso {P}hase {C}rystallization -- {A}
{M}ethod for the {S}tructural {I}nvestigation of {M}embrane
{P}roteins},
journal = {PLoS one},
volume = {7},
issn = {1932-6203},
address = {Lawrence, Kan.},
publisher = {PLoS},
reportid = {PreJuSER-111979},
pages = {e35458},
year = {2012},
note = {Record converted from VDB: 16.11.2012},
abstract = {We investigated in meso crystallization of membrane
proteins to develop a fast screening technology which
combines features of the well established classical vapor
diffusion experiment with the batch meso phase
crystallization, but without premixing of protein and
monoolein. It inherits the advantages of both methods,
namely (i) the stabilization of membrane proteins in the
meso phase, (ii) the control of hydration level and additive
concentration by vapor diffusion. The new technology (iii)
significantly simplifies in meso crystallization experiments
and allows the use of standard liquid handling robots
suitable for 96 well formats. CIMP crystallization
furthermore allows (iv) direct monitoring of phase
transformation and crystallization events. Bacteriorhodopsin
(BR) crystals of high quality and diffraction up to 1.3 Å
resolution have been obtained in this approach. CIMP and the
developed consumables and protocols have been successfully
applied to obtain crystals of sensory rhodopsin II (SRII)
from Halobacterium salinarum for the first time.},
keywords = {Bacteriorhodopsins: chemistry / Crystallization /
Crystallography, X-Ray: methods / Glycerides: chemistry /
Halobacterium salinarum / Halorhodopsins: chemistry /
Membrane Proteins: chemistry / Phase Transition / Protein
Stability / Sensory Rhodopsins: chemistry / Glycerides (NLM
Chemicals) / Halorhodopsins (NLM Chemicals) / Membrane
Proteins (NLM Chemicals) / Sensory Rhodopsins (NLM
Chemicals) / sensory rhodopsin II protein, archaeal (NLM
Chemicals) / monoolein (NLM Chemicals) / Bacteriorhodopsins
(NLM Chemicals)},
cin = {ICS-5 / ICS-6},
ddc = {500},
cid = {I:(DE-Juel1)ICS-5-20110106 / I:(DE-Juel1)ICS-6-20110106},
pnm = {BioSoft: Makromolekulare Systeme und biologische
Informationsverarbeitung / Funktion und Dysfunktion des
Nervensystems},
pid = {G:(DE-Juel1)FUEK505 / G:(DE-Juel1)FUEK409},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:22536388},
pmc = {pmc:PMC3334905},
UT = {WOS:000305336200043},
doi = {10.1371/journal.pone.0035458},
url = {https://juser.fz-juelich.de/record/111979},
}