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@ARTICLE{Ivanova:11309,
author = {Ivanova, M. and Ricote, S. and Meulenberg, W. A. and
Haugsrud, R. and Ziegner, M.},
title = {{E}ffects of {A}- and {B}-site (co-)acceptor doping on the
structure and proton conductivity of {L}a{N}b{O}4},
journal = {Solid state ionics},
volume = {213},
issn = {0167-2738},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {PreJuSER-11309},
pages = {45 - 52},
year = {2012},
note = {Record converted from VDB: 12.11.2012},
abstract = {B-site and A- and B-site co-doped lanthanum niobates,
La(1-x)DA(x)Nb(1-y)DB(y)O(4-delta), where D-A stands for Ca
or Ba and D-B for Ga, Ge or In (x = 0 or 0.01; y = 0.01),
have been synthesized via the solid-state route. Essentially
single-phase materials were obtained after 10 h at 1500
degrees C with monoclinic Fergusonite structure at room
temperature. The unit cell volume increases slightly with
the presence of the acceptor. The electrical conductivity of
the materials, characterized as a function of the
temperature from 300 degrees C to 900 degrees C under wet
reducing conditions with AC impedance spectroscopy, was
dominated by protons. The maximum conductivity of 4.1 .
10(-4) S . cm(-1) at 900 degrees C was obtained for
La0.99Ca0.01Nb0.99Ga0.01O4-delta, which is a factor of
similar to 2.5 lower than the highest conductivity reported
for the A-site Ca-doped LaNbO4. Based on a semi-quantitative
evaluation it was shown that the hydration of the B-site and
A- and B-site co-doped LaNbO4, is slightly more exothermic
and that the proton mobility has higher activation
enthalpies than Ca-doped LaNbO4. This is accounted for by a
stronger association between the acceptor and the proton for
B-site than for A-site doping. (c) 2011 Elsevier B.V. All
rights reserved.},
keywords = {J (WoSType)},
cin = {IEK-1},
ddc = {530},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {Rationelle Energieumwandlung},
pid = {G:(DE-Juel1)FUEK402},
shelfmark = {Chemistry, Physical / Physics, Condensed Matter},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000303636900010},
doi = {10.1016/j.ssi.2011.06.012},
url = {https://juser.fz-juelich.de/record/11309},
}