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@ARTICLE{Bland:11617,
author = {Bland, S.R. and Angst, M. and Adiga, S. and Scagnoli, V.
and Johnson, R.D. and Herrero-Martin, J. and Hatton, P.D.},
title = {{S}ymmetry and charge order in {F}e2{OBO}3 studied through
polarized resonant x-ray diffraction},
journal = {Physical review / B},
volume = {82},
number = {11},
issn = {1098-0121},
address = {College Park, Md.},
publisher = {APS},
reportid = {PreJuSER-11617},
pages = {115110},
year = {2010},
note = {The authors wish to thank the ESRF for the beamtime and
experimental support. S.R.B., R.D.J., and P.D.H. thank EPSRC
and STFC for funding. M.A. and S.A. acknowledge support by
the Initiative and Networking Fund of the Helmholtz
Association of German Research Centers through the
Helmholtz-University Young Investigator Group Complex
Ordering Phenomena in Multifunctional Oxides and by the
institute of scattering methods. S.R.B. thanks Y. Joly for
helpful discussions and assistance with FDMNES, and C. B.
Buckley for additional experimental support. The authors
thank R. P. Hermann for preliminary measurements and helpful
EXAFS discussions and results. This work was partially
performed on the EPSRC-funded XMaS beamline at the ESRF,
directed by M. J. Cooper and C. A. Lucas. We are grateful to
the beamline team of S. D. Brown, P. Normile, O. Bikondoa,
L. Bouchenoire, and P. Thompson for their invaluable
assistance, and to S. Beaufoy and J. Kervin for additional
support.},
abstract = {Bond valence sum calculations have previously suggested
that iron oxyborate exhibits charge order of the Fe ions
with integer 2+/3+ valence states. Meanwhile transition
metal oxides typically show much smaller, fractional charge
disproportionations. Using resonant x-ray diffraction at the
iron K edge, we find resonant features which are much larger
than those ordinarily observed in charge ordered oxides.
Simulations were subsequently performed using a
cluster-based, monoelectronic code. The nanoscale domain
structure prevents precise fitting; nevertheless the
simulations confirm the diagonal charge order symmetry, as
well as the unusually large charge disproportionation. We
have demonstrated the conversion of linearly to nonlinearly
polarized light and vice versa through full polarization
analysis. Simulations show that this effect principally
results from interference between the isotropic and
anisotropic scattering terms. This mechanism is likely to
account for similar observations in alternative systems.},
keywords = {J (WoSType)},
cin = {IFF-4 / IFF-5 / JARA-FIT / Jülich Centre for Neutron
Science JCNS (JCNS) ; JCNS},
ddc = {530},
cid = {I:(DE-Juel1)VDB784 / I:(DE-Juel1)VDB785 /
$I:(DE-82)080009_20140620$ / I:(DE-Juel1)JCNS-20121112},
pnm = {Großgeräte für die Forschung mit Photonen, Neutronen und
Ionen (PNI) / BioSoft: Makromolekulare Systeme und
biologische Informationsverarbeitung},
pid = {G:(DE-Juel1)FUEK415 / G:(DE-Juel1)FUEK505},
shelfmark = {Physics, Condensed Matter},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000281723100002},
doi = {10.1103/PhysRevB.82.115110},
url = {https://juser.fz-juelich.de/record/11617},
}