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@ARTICLE{Li:12063,
author = {Li, X. and Zamponi, M. and Hong, K. and Porcar, L. and
Shew, C.-Y. and Jenkins, T. and Liu, E. and Smith, G.S. and
Herwig, K.W. and Liu, Y. and Chen, W.-R.},
title = {p{H} {R}esponsiveness of {P}olyelectrolyte {D}endrimers:
{A} {D}ynamical {P}erspective},
journal = {Soft matter},
volume = {7},
issn = {1744-683X},
address = {Cambridge},
publisher = {Royal Society of Chemistry (RSC)},
reportid = {PreJuSER-12063},
pages = {618 - 622},
year = {2011},
note = {This research at Oak Ridge National Laboratory's SNS was
sponsored by the Scientific User Facilities Division, Office
of Basic Energy Sciences, U.S. Department of Energy. CNMS is
sponsored at ORNL by the Division of Scientific User
Facilities, U.S. Department of Energy.},
abstract = {A combined quasi-elastic neutron scattering (QENS) and
high-resolution solution NMR spectroscopy study was
conducted to investigate the internal dynamics of aqueous
(D2O) G5 PAMAM dendrimer solutions as a function of
molecular protonation at room temperature. Localized motion
of the dendrimer segments was clearly exhibited in the QENS
data analysis while the global, center-of-mass translational
diffusion was measured by NMR. Our results unambiguously
demonstrate an increased rapidity in local scale (similar to
3 angstrom) motion upon increasing the molecular
protonation. This is contrary to an intuitive picture that
increased charge stiffens the dendrimer segments thereby
inhibiting local motion. These charge-induced changes may be
a result of interactions with the surrounding counterions
and water molecules as the segments explore additional
intra-dendrimer volume made available by slight
electrostatic swelling and redistribution of mass in the
dendrimer interior. This observation is relevant to
development of a microscopic picture of dendrimer-based
packages as guest-molecule delivery vehicles because
reorganization of the confining dendrimer segments must be a
precursor to guest-molecule release.},
keywords = {J (WoSType)},
cin = {PGI-4 / ICS-1 / Jülich Centre for Neutron Science JCNS
(JCNS) ; JCNS},
ddc = {530},
cid = {I:(DE-Juel1)PGI-4-20110106 / I:(DE-Juel1)ICS-1-20110106 /
I:(DE-Juel1)JCNS-20121112},
pnm = {BioSoft: Makromolekulare Systeme und biologische
Informationsverarbeitung / Großgeräte für die Forschung
mit Photonen, Neutronen und Ionen (PNI)},
pid = {G:(DE-Juel1)FUEK505 / G:(DE-Juel1)FUEK415},
shelfmark = {Chemistry, Physical / Materials Science, Multidisciplinary
/ Physics, Multidisciplinary / Polymer Science},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000286110900038},
doi = {10.1039/c0sm00671h},
url = {https://juser.fz-juelich.de/record/12063},
}