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@ARTICLE{Komsiyska:128631,
      author       = {Komsiyska, L. and Staikov, G.},
      title        = {{E}lectrocrystallization of {A}u nanoparticles on glassy
                      carbon from {HC}l{O}$_{4}$ solution containing
                      [{A}u{C}l$_{4}$]−},
      journal      = {Electrochimica acta},
      volume       = {54},
      number       = {2},
      issn         = {0013-4686},
      address      = {New York, NY [u.a.]},
      publisher    = {Elsevier},
      reportid     = {FZJ-2013-00365},
      pages        = {168 - 172},
      year         = {2008},
      abstract     = {The mechanism and kinetics of electrocrystallization of Au
                      nanoparticles on glassy carbon (GC) were investigated in the
                      system GC/1 mM KAuCl4 + 0.1 M HClO4. Experimental results
                      show that the gold electrodeposition follows the so-called
                      Volmer–Weber growth mechanism involving formation and
                      growth of 3D Au nanoparticles on an unmodified GC substrate.
                      The analysis of current transients shows that at relatively
                      positive electrode potentials (E ≥ 0.84 V) the deposition
                      kinetics corresponds to the theoretical model for
                      progressive nucleation and diffusion-controlled 3D growth of
                      Au nanoparticles. The potential dependence of the nucleation
                      rate extracted from the current transients is in agreement
                      with the atomistic theory of nucleation. At sufficiently
                      negative electrode potentials (E ≤ 0.64 V) the nucleation
                      frequency becomes very high and the nucleation occurs
                      instantaneously. Based on this behaviour is applied a
                      potentiostatic double-pulse routine, which allows controlled
                      electrodeposition of Au nanoparticles with a relatively
                      narrow size distribution.},
      cin          = {PGI-3 / JARA-FIT},
      ddc          = {540},
      cid          = {I:(DE-Juel1)PGI-3-20110106 / $I:(DE-82)080009_20140620$},
      pnm          = {142 - Controlling Spin-Based Phenomena (POF3-142)},
      pid          = {G:(DE-HGF)POF3-142},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000263282400003},
      doi          = {10.1016/j.electacta.2008.08.013},
      url          = {https://juser.fz-juelich.de/record/128631},
}