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@PHDTHESIS{Steitz:129276,
author = {Steitz, Bettina},
title = {{E}xperimental determination of the partitioning
coefficient of nopinone as a marker substance in organic
aerosol},
volume = {169},
school = {Universität Wuppertal},
type = {Dissertation},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2013-00792},
isbn = {978-3-89336-862-4},
series = {Schriften des Forschungszentrums Jülich : Energie $\&$
Umwelt / Energy $\&$ Environment},
pages = {132 p.},
year = {2013},
note = {Dissertation, Universität Wuppertal, 2012},
abstract = {Atmospheric aerosols have a significant influence on the
radiation budget and chemical processes in the atmosphere.
Thus, they have an impact on climate. They are relevant in
many environmental processes and influence human health. In
many regions, secondary organic aerosol (SOA) makes a major
contribution to the total aerosol mass. Therefore, SOA
significantly influences aerosol properties. The complex and
versatile chemical composition of SOA makes the analysis of
its formation and chemical behavior difficult and thus
complicates global and local climate modeling. One major
issue in current models is the prediction of the organic
matter in the atmosphere. For this, a detailed understanding
of SOA formation from volatile organic compounds (VOCs) is
of importance. VOCs undergo oxidation in the atmosphere
which results in the formation of semivolatile organic
compounds. These partition between the gas and the particle
phase. The compoundspecific gas-to-particle partitioning can
be described with the temperature-dependent partitioning
coefficient. This work is dedicated to its experimental
determination. To this end, a new measurement technique for
compound-specific analysis of organic aerosol was used. The
Aerosol Collection Module (ACM) is a newly developed
instrument which collects aerosol particles, converts them
into the gas phase via thermal desorption and transfers them
to a gas phase detector for further analysis. In this work,
the ACM was coupled to a high-resolution Proton Transfer
Reaction-Time of Flight-Mass Spectrometer (PTR-ToF-MS)for
the first time and used in $\alpha$ -, and $\beta$-pinene
ozonolysis experiments at the AIDA chamber of the Karlsruhe
Institute of Technology (KIT). For the data analysis,
routines were developed based on Aerosol Mass Spectrometer
(AMS) data analysis. The partitioning coefficient of
nopinone, as the major $\beta$-pinene ozonolysis product,
and its temperature dependence was determined. For this
purpose, two experimental approaches were employed: the
coupling of ACM and PTR-ToF-MS, and measurements using the
PTRToF- MS with and without particle filter. The temperature
dependence of the partitioning coefficient derived from ACM
and PTR-ToF-MS was comparable to the theoretical temperature
dependence found in literature. A comparison with calculated
partitioning coefficients following theory showed that the
experimental partitioning coefficients of this work were
about one order of magnitude higher. This leads to the
conclusion that the amount of nopinone in the aerosol
particle phase is underestimated by theory. As literature on
experimentally derived partitioning coefficients is sparse,
further investigations of the partitioning coefficient of
other substances with the combination of ACM and PTR-ToF-MS
could help to improve the understanding of SOA formation
and, thus, SOA prediction.},
keywords = {Dissertation (GND)},
cin = {IEK-8},
cid = {I:(DE-Juel1)IEK-8-20101013},
pnm = {233 - Trace gas and aerosol processes in the troposphere
(POF2-233)},
pid = {G:(DE-HGF)POF2-233},
typ = {PUB:(DE-HGF)3 / PUB:(DE-HGF)11},
url = {https://juser.fz-juelich.de/record/129276},
}