000001353 001__ 1353
000001353 005__ 20180208233931.0
000001353 0247_ $$2pmid$$apmid:18414833
000001353 0247_ $$2DOI$$a10.1007/s00216-008-2081-1
000001353 0247_ $$2WOS$$aWOS:000255996900040
000001353 037__ $$aPreJuSER-1353
000001353 041__ $$aeng
000001353 082__ $$a540
000001353 084__ $$2WoS$$aBiochemical Research Methods
000001353 084__ $$2WoS$$aChemistry, Analytical
000001353 1001_ $$0P:(DE-HGF)0$$aFörster, M.$$b0
000001353 245__ $$aAnalysis of aged sulfadiazine residues in soils using microwave extraction and liquid  chromatagraphy tandem mass spectrometry
000001353 260__ $$aBerlin$$bSpringer$$c2008
000001353 300__ $$a1029 - 1038
000001353 3367_ $$0PUB:(DE-HGF)16$$2PUB:(DE-HGF)$$aJournal Article
000001353 3367_ $$2DataCite$$aOutput Types/Journal article
000001353 3367_ $$00$$2EndNote$$aJournal Article
000001353 3367_ $$2BibTeX$$aARTICLE
000001353 3367_ $$2ORCID$$aJOURNAL_ARTICLE
000001353 3367_ $$2DRIVER$$aarticle
000001353 440_0 $$08664$$aAnalytical and Bioanalytical Chemistry$$v391$$x1618-2642
000001353 500__ $$aRecord converted from VDB: 12.11.2012
000001353 520__ $$aAn efficient extraction of sulfadiazine residues from soils is difficult, as sulfadiazine is known to form quickly sequestering residues. The objective of this study was to optimize an exhaustive extraction for aged residues of sulfadiazine and its two major metabolites, N-acetylsulfadiazine and 4-hydroxysulfadiazine, from soil. For this purpose two representative used agricultural soils (Luvisol, Cambisol) were blended with manure derived from [(14)C]sulfadiazine-treated pigs and incubated at 10 degrees C in the laboratory. After different extraction tests with various solvent mixtures (two- to four-component mixtures with water, methanol, acetonitrile, acetone, and/or ethyl acetate), different pH values (pH 4 and 9), and extraction temperatures (up to 200 degrees C), soil extracts were measured by liquid scintillation counting and liquid chromatography coupled to tandem mass spectrometry. With respect to sulfadiazine yields, stability of soil extracts, and the amount of coextracted matrix, a microwave extraction of soil (15 min, 150 degrees C) using acetonitrile/water 1:4 (v/v) is the method of choice for the exhaustive extraction of aged sulfadiazine residues from soils.
000001353 536__ $$0G:(DE-Juel1)FUEK407$$2G:(DE-HGF)$$aTerrestrische Umwelt$$cP24$$x0
000001353 588__ $$aDataset connected to Web of Science, Pubmed
000001353 650_2 $$2MeSH$$aChromatography, High Pressure Liquid: methods
000001353 650_2 $$2MeSH$$aMicrowaves
000001353 650_2 $$2MeSH$$aReproducibility of Results
000001353 650_2 $$2MeSH$$aSoil: analysis
000001353 650_2 $$2MeSH$$aSolid Phase Extraction: methods
000001353 650_2 $$2MeSH$$aSulfadiazine: analysis
000001353 650_2 $$2MeSH$$aSulfadiazine: radiation effects
000001353 650_2 $$2MeSH$$aTandem Mass Spectrometry: methods
000001353 650_7 $$00$$2NLM Chemicals$$aSoil
000001353 650_7 $$068-35-9$$2NLM Chemicals$$aSulfadiazine
000001353 650_7 $$2WoSType$$aJ
000001353 65320 $$2Author$$amicrowave extraction
000001353 65320 $$2Author$$asulfadiazine
000001353 65320 $$2Author$$ametabolites
000001353 65320 $$2Author$$asoil
000001353 65320 $$2Author$$amanure
000001353 65320 $$2Author$$aaging
000001353 7001_ $$0P:(DE-HGF)0$$aLaabs, V.$$b1
000001353 7001_ $$0P:(DE-HGF)0$$aLamshöft, M.$$b2
000001353 7001_ $$0P:(DE-Juel1)VDB2346$$aPütz, T.$$b3$$uFZJ
000001353 7001_ $$0P:(DE-HGF)0$$aAmerlung, W.$$b4
000001353 773__ $$0PERI:(DE-600)1459122-4$$a10.1007/s00216-008-2081-1$$gVol. 391, p. 1029 - 1038$$p1029 - 1038$$q391<1029 - 1038$$tAnalytical and bioanalytical chemistry$$v391$$x1618-2642$$y2008
000001353 8567_ $$uhttp://dx.doi.org/10.1007/s00216-008-2081-1
000001353 909CO $$ooai:juser.fz-juelich.de:1353$$pVDB
000001353 9131_ $$0G:(DE-Juel1)FUEK407$$bErde und Umwelt$$kP24$$lTerrestrische Umwelt$$vTerrestrische Umwelt$$x0
000001353 9141_ $$y2008
000001353 915__ $$0StatID:(DE-HGF)0010$$aJCR/ISI refereed
000001353 9201_ $$0I:(DE-Juel1)VDB793$$d31.10.2010$$gICG$$kICG-4$$lAgrosphäre$$x1
000001353 970__ $$aVDB:(DE-Juel1)102407
000001353 980__ $$aVDB
000001353 980__ $$aConvertedRecord
000001353 980__ $$ajournal
000001353 980__ $$aI:(DE-Juel1)IBG-3-20101118
000001353 980__ $$aUNRESTRICTED
000001353 981__ $$aI:(DE-Juel1)IBG-3-20101118