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@TECHREPORT{Schnfeld:136158,
author = {Schönfeld, B.},
title = {{U}ntersuchung von {F}renkeldefekten in
tieftemperaturbestrahlten {HCP} {K}ristallen mit {H}ilfe der
diffusen {R}öntgenstreuung. 1650},
volume = {1650},
number = {Juel-1650},
address = {Jülich},
publisher = {Kernforschungsanlage Jülich},
reportid = {PreJuSER-136158, Juel-1650},
series = {Berichte der Kernforschungsanlage Jülich},
pages = {88 S.},
year = {1980},
note = {Record converted from JUWEL: 18.07.2013},
abstract = {Single crystals of 3 hexagonal metals (Zn, Cd, Mg) were
irradiated at 4.5K with 3MeV electrons up to doses of $\sim
10^{19}$ $e^{-}$/cm$^{2}$. The irradiation induced defects
were investigated by measurements of the Huang diffuse
scattering of X-rays, the lattice parameter change and the
electrical resistivity change. Only for Zn a random
distribution of single interstitial atoms (S.I.A.) and
vacancies was found. The S.I.A. was characterized by a large
relaxation volume of (3.6±0.7) atomic volumes and a strong
anisotropy of the defect displacement field. Consistent with
a dumbbell configuration of the S.I.A. the large
displacement was along the c-axis. The contribution of a
Frenkel defect to the electrical resistivity change was
$\rho_{F}$ = (15.3±5.7) $\mu \Omega$cm/at\%. For Cd
interstitial agglomerates of <10 interstitials were found.
Their size increased with the irradiation dose. This
indicated interstitial mobility at the irradiation
temperature. For Mg interstitial agglomerates of 2-3
interstitials were observed. It was shown, that these
agglomerates were formed by interstitial migration during
irradiation, similar to Cd. In contrast to Cd, no dose
dependence of their size was found. This unique behaviour
was tentatively explained by the existence of a nucleation
barrier. During thermal annealing in stage II small
interstitial agglomerates of ~10 interstitials were found
for all 3 metals. In the case of Zn and Cd (c/a $\approx$
1.85) they seem to nucleate and grow on the basal plane, in
the case of Mg (c/a $\approx$ 1.6) however, on prismatic
planes.},
cin = {IFF},
cid = {I:(DE-Juel1)VDB241},
shelfmark = {FHCF - Defect characterization / FHCB - X-ray scattering /
FDFC - Radiation effects in metals, nuclear radiation
effects},
typ = {PUB:(DE-HGF)29},
url = {https://juser.fz-juelich.de/record/136158},
}