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@ARTICLE{Vad:13982,
author = {Vad, T. and Sager, W.F.C.},
title = {{C}omparison of iterative desmearing procedures for
one-dimensional small-angle scattering data},
journal = {Journal of applied crystallography},
volume = {44},
issn = {0021-8898},
address = {Copenhagen},
publisher = {Munksgaard},
reportid = {PreJuSER-13982},
pages = {32 - 42},
year = {2011},
note = {The authors thank Dr Aurel Radulescu (Julich Centre for
Neutron Science, Forschungszentrum Julich) for experimental
assistance at the KWS-2 beamline, Dr Johan Buitenhuis
(Institut fur Festkorperforschung, Forschungszentrum Julich)
for providing the silica sample, and one of the referees for
his/her valuable comments. Financial support by the
Bundesministerium fur Bildung und Forschung, grant No.
05KS7OD2, is gratefully acknowledged.},
abstract = {Two simple iterative desmearing procedures - the Lake
algorithm and the Van Cittert method - have been
investigated by introducing different convergence criteria
using both synthetic and experimental small-angle neutron
scattering data. Implementing appropriate convergence
criteria resulted in stable and reliable solutions in
correcting resolution errors originating from instrumental
smearing, i.e. finite collimation and polychromaticity of
the incident beam. Deviations at small momentum transfer for
concentrated ensembles of spheres encountered in earlier
studies are not observed. Amplification of statistical
errors can be reduced by applying a noise filter after
desmearing. In most cases investigated, the modified Lake
algorithm yields better results with a significantly smaller
number of iterations and is, therefore, suitable for
automated desmearing of large numbers of data sets.},
keywords = {J (WoSType)},
cin = {ICS-3},
ddc = {540},
cid = {I:(DE-Juel1)ICS-3-20110106},
pnm = {BioSoft: Makromolekulare Systeme und biologische
Informationsverarbeitung},
pid = {G:(DE-Juel1)FUEK505},
experiment = {EXP:(DE-MLZ)KWS2-20140101},
shelfmark = {Crystallography},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000286475300005},
doi = {10.1107/S0021889810049721},
url = {https://juser.fz-juelich.de/record/13982},
}