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@PHDTHESIS{Lennartz:14152,
author = {Lennartz, Maria Christina},
title = {{A}lternative systems for molecular electronics:
functionalized carboxylic acids on structured surfaces},
volume = {13},
school = {RWTH Aachen},
type = {Dr. (Univ.)},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {PreJuSER-14152},
isbn = {978-3-89336-667-5},
series = {Schriften des Forschungszentrums Jülich. Reihe Information
/ Information},
pages = {183 S.},
year = {2010},
note = {Record converted from JUWEL: 18.07.2013; RWTH Aachen,
Diss., 2010},
abstract = {Molecular electronics is recognized as a key candidate to
succeed the silicon based technology as soon as the end of
the semiconductor roadmap is reached. An important step
towards the realization of molecular electronics is the
combination of common CMOS devices and molecular elements to
new systems. Today, an advantageously used metal for wires
and interconnects in electronic industry is copper due to
its low resistance. Thus, it is essential to get a
fundamental understanding of organic/copper interfaces and
to combine functional molecular systems with linkers which
are copper sensitive. Within the scope of this work,
carboxylate molecules were investigated which chemically
bind to copper. They self-assemble in highly ordered
monolayer structures on, e.g., Cu(110) surfaces. Main task
of this work is the electronic characterization of the
combined molecule/metal system as well as the systematic
investigation of the influence of specific molecular parts
on the electronic transport. Scanning tunneling microscopy
(STM) was used as main technique to investigate the
topographic and electronic structures throughout the study,
but complementary techniques like XPS/AES, LEED and UV-VIS
spectroscopy were employed as well to get additional
information. The transport properties were investigated by
current-voltage (I-V) and current-distance (I-z)
spectroscopy. Distance-dependent I-V measurements enable the
detection of the density of states of the system with the
orbital energies appearing as peaks in the dI/dV curves.
Density functional theory based calculations (IFF-1, FZ
Jülich) were used to assign the measured peaks to specific
molecular orbitals. Thus, it is possible to display the
molecular orbitals with respect to their energies and their
spatial distribution. A detailed analysis of all
experimentally probed molecular orbitals has shown that the
calculated LDOS represents a characteristic fingerprint
corresponding to the substitution pattern of the
carboxylates bonded to Cu(110). It was shown that, e.g.,
nitrogen heteroatoms cause a shift in the molecular orbital
energies and lead to a system with smaller HOMO-LUMO gap.
With a detailed knowledge of the system parameters it is now
possible to make precise theoretical predictions on the
transport properties of other carboxylate species. Thus, a
first toolbox is composed which allows to combine molecular
moieties to build up a molecule linked to a metallic
electrode with a designed functionality. In a second step
carboxylates with a second functional group were
investigated. These molecules chemically bind to two
different electrode materials, e.g., with one side of the
molecule to copper and with the other side to gold. This
causes a diode functionality of the molecule within the
junction. The molecular self-assembly of these molecules
(here TMBA) was investigated on Au(111) surfaces. STM
investigations show ordered monolayer structures and XPS
measurements confirm a nondestructive chemisorption of the
molecules. The electron transport properties of the system
could be revealed from I-V measurements by monitoring the
local density of states as well as from I-z measurements by
calculating the molecule specific tunneling decay constant
$\beta$. Finally, a short excursion presents an alternative
approach to combine molecules with CMOS materials. This
approach does not use the metal layer as linking point but
the semiconductor areas. Semiconductor surfaces, like
Ge(001), with self-assembled metallic Pt nanowires build a
highly ordered 1D nanotemplate for the selective assembly of
triphenylphosphane molecules.},
cin = {IFF-6 / JARA-FIT},
ddc = {500},
cid = {I:(DE-Juel1)VDB786 / $I:(DE-82)080009_20140620$},
pnm = {Grundlagen für zukünftige Informationstechnologien},
pid = {G:(DE-Juel1)FUEK412},
typ = {PUB:(DE-HGF)11 / PUB:(DE-HGF)3},
url = {https://juser.fz-juelich.de/record/14152},
}