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000014189 084__ $$2WoS$$aPhysics, Atomic, Molecular & Chemical
000014189 1001_ $$0P:(DE-Juel1)VDB96975$$aSchneider, G.J.$$b0$$uFZJ
000014189 245__ $$aCorrelation of mass fractal dimension and cluster size of silica in styrene butadiene rubber composites
000014189 260__ $$aMelville, NY$$bAmerican Institute of Physics$$c2010
000014189 300__ $$a094902
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000014189 440_0 $$022061$$aJournal of Chemical Physics$$v133$$x0021-9606
000014189 500__ $$aWe are grateful to the HASYLAB/DESY (Hamburg, Germany) for the beam time on BW4 and for the financial support and to the beam line staff, R. Dohrmann, M. Dommach, and Rainer Gehrke, for help and technical assistance.
000014189 520__ $$aThe morphology of the precipitated silica VN3 filled in styrene butadiene rubber was studied as a function of the volume fraction Φ by means of small-angle X-ray scattering experiments. The wide q-range of 0.008 nm(-1)<q<1 nm(-1) probes the structures of the primary particles, the clusters, and resolves a part of the larger clusters of the silica. The diameter of the primary particles and their surface roughness are independent from the silica concentration. The size of the clusters and the corresponding aggregation number depend on Φ. This observation could be ascribed to external mechanical forces because of the mixing process and to growing cluster-cluster interactions with increasing filler fraction. In contrast the mass fractal dimension does not depend on Φ, and by that means experimentally proving that there is not necessarily a correlation between the mass fractal dimension and the cluster size.
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000014189 65320 $$2Author$$aaggregation
000014189 65320 $$2Author$$afilled polymers
000014189 65320 $$2Author$$afractals
000014189 65320 $$2Author$$amixing
000014189 65320 $$2Author$$ananoparticles
000014189 65320 $$2Author$$arubber
000014189 65320 $$2Author$$asilicon compounds
000014189 65320 $$2Author$$asurface roughness
000014189 65320 $$2Author$$aX-ray scattering
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000014189 7001_ $$0P:(DE-HGF)0$$aVollnhals, V.$$b1
000014189 7001_ $$0P:(DE-HGF)0$$aBrandt, K.$$b2
000014189 7001_ $$0P:(DE-HGF)0$$aRoth, S.V.$$b3
000014189 7001_ $$0P:(DE-HGF)0$$aGöritz, D.$$b4
000014189 773__ $$0PERI:(DE-600)1473050-9$$a10.1063/1.3469827$$gVol. 133, p. 094902$$p094902$$q133<094902$$tThe @journal of chemical physics$$v133$$x0021-9606$$y2010
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