000014703 001__ 14703
000014703 005__ 20240619090949.0
000014703 0247_ $$2DOI$$a10.1107/S0021889810053823
000014703 0247_ $$2WOS$$aWOS:000288758500014
000014703 0247_ $$2MLZ$$aBusch:ce5108
000014703 037__ $$aPreJuSER-14703
000014703 041__ $$aeng
000014703 082__ $$a540
000014703 084__ $$2WoS$$aCrystallography
000014703 1001_ $$0P:(DE-Juel1)VDB7313$$aBusch, P.$$b0$$uFZJ
000014703 245__ $$aDebye-Scherrer rings from block copolymer films with power-like order
000014703 260__ $$aCopenhagen$$bMunksgaard$$c2011
000014703 300__ $$a370 - 379
000014703 3367_ $$0PUB:(DE-HGF)16$$2PUB:(DE-HGF)$$aJournal Article
000014703 3367_ $$2DataCite$$aOutput Types/Journal article
000014703 3367_ $$00$$2EndNote$$aJournal Article
000014703 3367_ $$2BibTeX$$aARTICLE
000014703 3367_ $$2ORCID$$aJOURNAL_ARTICLE
000014703 3367_ $$2DRIVER$$aarticle
000014703 440_0 $$03041$$aJournal of Applied Crystallography$$v44$$x0021-8898$$y2
000014703 500__ $$aCHESS is a national user facility supported by the National Science Foundation and the National Institutes of Health/National Institute of General Medical Sciences under award No. DMR-0225180. We thank Sita Krishnan for the preparation of the semifluorinated diblock copolymer sample. PMB acknowledges financial support by the Deutsche Forschungsgemeinschaft in project No. MU1487/6.
000014703 520__ $$aThe powder-like orientation of lamellar domains in thin films of the diblock copolymer polystyrene-block-poly(methyl methacrylate) is investigated using grazing-incidence small-angle X-ray scattering (GISAXS) and grazing-incidence small-angle neutron scattering (GISANS). Conventional monochromatic GISANS and GISAXS measurements are compared with neutron time-of-flight GISANS. For angles of incidence and exit larger than the critical angle of total external reflection of the polymer, Debye-Scherrer rings are observed. The position of the Debye-Scherrer rings is described quantitatively based on a reduced version of the distorted-wave Born approximation. A strong distortion of the ring shape is caused by refraction and reflections from the film interfaces. Close to the critical angle, the ring shape collapses into a banana shape.
000014703 536__ $$0G:(DE-Juel1)FUEK505$$2G:(DE-HGF)$$aBioSoft: Makromolekulare Systeme und biologische Informationsverarbeitung$$cP45$$x0
000014703 536__ $$0G:(DE-Juel1)FUEK415$$2G:(DE-HGF)$$aGroßgeräte für die Forschung mit Photonen, Neutronen und Ionen (PNI)$$cP55$$x1
000014703 588__ $$aDataset connected to Web of Science
000014703 65320 $$2Author$$agrazing-incidence small-angle scattering
000014703 65320 $$2Author$$aGISANS
000014703 65320 $$2Author$$aGISAXS
000014703 65320 $$2Author$$apowder diffraction
000014703 65320 $$2Author$$adistorted-wave Born approximation
000014703 65320 $$2Author$$athin films
000014703 65320 $$2Author$$adiblock copolymer
000014703 650_7 $$2WoSType$$aJ
000014703 65027 $$0V:(DE-MLZ)SciArea-210$$2V:(DE-HGF)$$aSoft Condensed Matter$$x0
000014703 65017 $$0V:(DE-MLZ)GC-2004-2016$$2V:(DE-HGF)$$aBasic research$$x1
000014703 65017 $$0V:(DE-MLZ)GC-180$$2V:(DE-HGF)$$aOthers$$x0
000014703 693__ $$0EXP:(DE-MLZ)KWS2-20140101$$1EXP:(DE-MLZ)FRMII-20140101$$5EXP:(DE-MLZ)KWS2-20140101$$6EXP:(DE-MLZ)NL3ao-20140101$$aForschungs-Neutronenquelle Heinz Maier-Leibnitz$$eKWS-2: Small angle scattering diffractometer$$fNL3ao$$x0
000014703 693__ $$0EXP:(DE-MLZ)REFSANS-20140101$$1EXP:(DE-MLZ)FRMII-20140101$$5EXP:(DE-MLZ)REFSANS-20140101$$6EXP:(DE-MLZ)NL2b-20140101$$aForschungs-Neutronenquelle Heinz Maier-Leibnitz$$eREFSANS: Horizontal TOF Reflectometer with GISANS option$$fNL2b$$x1
000014703 7001_ $$0P:(DE-HGF)0$$aRauscher, M.$$b1
000014703 7001_ $$0P:(DE-HGF)0$$aMoulin, J.-F.$$b2
000014703 7001_ $$0P:(DE-HGF)0$$aMüller-Buschbaum, P.$$b3
000014703 773__ $$0PERI:(DE-600)2020879-0$$a10.1107/S0021889810053823$$gVol. 44, p. 370 - 379$$p370 - 379$$q44<370 - 379$$tJournal of applied crystallography$$v44$$x0021-8898$$y2011
000014703 8567_ $$uhttp://dx.doi.org/10.1107/S0021889810053823
000014703 909CO $$ooai:juser.fz-juelich.de:14703$$pVDB$$pVDB:MLZ
000014703 915__ $$0StatID:(DE-HGF)0010$$aJCR/ISI refereed
000014703 9141_ $$y2011
000014703 9131_ $$0G:(DE-Juel1)FUEK505$$aDE-HGF$$bSchlüsseltechnologien$$kP45$$lBiologische Informationsverarbeitung$$vBioSoft: Makromolekulare Systeme und biologische Informationsverarbeitung$$x0
000014703 9131_ $$0G:(DE-Juel1)FUEK415$$aDE-HGF$$bStruktur der Materie$$kP55$$lGroßgeräteforschung mit Photonen, Neutronen und Ionen$$vGroßgeräte für die Forschung mit Photonen, Neutronen und Ionen (PNI)$$x1
000014703 9132_ $$0G:(DE-HGF)POF3-623$$1G:(DE-HGF)POF3-620$$2G:(DE-HGF)POF3-600$$aDE-HGF$$bForschungsbereich Materie$$lIn-house research on the structure, dynamics and function of matter$$vNeutrons for Research on Condensed Matter$$x0
000014703 9201_ $$0I:(DE-Juel1)PGI-4-20110106$$gPGI$$kPGI-4$$lStreumethoden$$x0
000014703 9201_ $$0I:(DE-Juel1)JCNS-FRM-II-20110218$$kJCNS (München) ; Jülich Centre for Neutron Science JCNS (München) ; JCNS-FRM-II$$lJCNS-FRM-II$$x1
000014703 9201_ $$0I:(DE-Juel1)JCNS-1-20110106$$gJCNS$$kJCNS-1$$lNeutronenstreuung$$x2
000014703 9201_ $$0I:(DE-Juel1)JCNS-2-20110106$$gJCNS$$kJCNS-2$$lStreumethoden$$x3
000014703 970__ $$aVDB:(DE-Juel1)127079
000014703 980__ $$aVDB
000014703 980__ $$aConvertedRecord
000014703 980__ $$ajournal
000014703 980__ $$aI:(DE-Juel1)PGI-4-20110106
000014703 980__ $$aI:(DE-Juel1)JCNS-FRM-II-20110218
000014703 980__ $$aI:(DE-Juel1)JCNS-1-20110106
000014703 980__ $$aI:(DE-Juel1)JCNS-2-20110106
000014703 980__ $$aUNRESTRICTED
000014703 981__ $$aI:(DE-Juel1)JCNS-2-20110106
000014703 981__ $$aI:(DE-Juel1)JCNS-FRM-II-20110218
000014703 981__ $$aI:(DE-Juel1)JCNS-2-20110106