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@PHDTHESIS{Frielinghaus:150421,
author = {Frielinghaus, Robert Detrich},
title = {{S}tructural influences on electrical transport in
nanostructures},
volume = {60},
school = {Universität Duisburg},
type = {Dr.},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2014-00480},
isbn = {978-3-89336-867-9},
series = {Schriften des Forschungszentrums Jülich. Reihe
Schlüsseltechnologien / Key Technologies},
pages = {VIII, 190 S.},
year = {2013},
note = {Universität Duisburg, Diss., 2013},
abstract = {The interplay between the molecular configuration and the
electrical and optical properties of various individual
nanostructures is studied in this thesis. These are carbon
nanotubes (CNTs), tetramanganese-decorated carbon nanotubes,
and InAs nanowires that are investigated on the
single-device level with high-resolution transmission
electron microscopy and spectroscopy (HR-TEM), Raman
scattering, and low-temperature quantum transport
measurements. These techniques probe complementary material
properties and can jointly provide a comprehensive
characterization of the individual nanostructure. This
correlation is achieved on a novel sample design developed
in the course of this thesis. It combines various
lithographic steps on a TEM membrane and is compatible with
many (self-assembled) nanostructures. It decouples the
device from the substrate, leading to clean transport
properties. An individual triple-walled carbon nanotube, as
identified using HR-TEM, is investigated with Raman
spectroscopy and room-temperature electrical transport. The
optical response and the transport channel can be assigned
to the individual walls. Quantum transport experiments are
performed on two additional carbon nanotube devices,
identified with the HR-TEM as a two-fold bundle of
single-walled CNTs and a triplewalled CNT, respectively. The
stability diagrams exhibit complex features as avoided
crossings, Fano-shaped coulomb peaks, and regular saw tooth
patterns. Their origin is only found with the detailed
knowledge of about the atomic structure. More precisely,
these features can be modeled with capacitive and molecular
interactions between the various elements of the devices and
the environment. Universal conductance fluctuations and the
phase-coherence length of four individual InAs nanowire
transport devices are likewise studied. Two different
temperature dependences can be measured. They are not
related to a crystal phase mixing because all four nanowires
are statistically identical in these terms as determined by
a HR-TEM measurement. The properties of carbon nanotubes can
be modified by chemical functionalization. The route
proposed in this thesis is the decoration with a
tetramanganese molecular antiferromagnet via a carboxylate
ligand exchange with the carbon nanotube. The degree of
functionalization can be controlled with the oxidation of
the CNT. The decoration is monitored with bright- and dark
field HR-TEM as well as energy-dispersive X-ray and electron
energy loss spectroscopy that show the repartition of the Mn
on the carbon nanotubes. Raman spectroscopy and SQUID
measurements provide further evidence of a successful
decoration and show the integrity of the hybrids. Transport
experiments on functionalized carbon nanotube networks
demonstrate the integrability of such structures into
single-hybrid quantum transport devices. In conclusion, the
developed sample layout has a great potential to investigate
the impact of specific structural modifications on optical
and electrical properties of individual nanostructures. This
is an important ingredient for the comparison of theoretical
predictions and experimental results.},
keywords = {Dissertation (GND)},
cin = {PGI-6},
ddc = {537.6226},
cid = {I:(DE-Juel1)PGI-6-20110106},
pnm = {422 - Spin-based and quantum information (POF2-422)},
pid = {G:(DE-HGF)POF2-422},
typ = {PUB:(DE-HGF)11},
url = {https://juser.fz-juelich.de/record/150421},
}