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@ARTICLE{Adelsberger:15283,
author = {Adelsberger, J. and Meier-Koll, A. and Bivigou-Koumba, A.M.
and Busch, P. and Holderer, O. and Hellweg, T. and
Laschewsky, A. and Müller-Buschbaum, P and Papadakis, C.M.},
title = {{T}he collapse transition and the segmental dynamics in
concentrated micellar solutions of {P}({S}-b-{NIPAM})
diblock copolymers},
journal = {Colloid and Polymer Science},
volume = {289},
issn = {0303-402x},
address = {Berlin},
publisher = {Springer},
reportid = {PreJuSER-15283},
year = {2011},
note = {We kindly acknowledge the given beam time by the Julich
Centre for Neutron Science at FRM II. This work was
supported by the DFG priority program SPP1259 "Intelligente
Hydrogele" (Pa771/4, Mu1487/8, La611/7, He2995/2). A.M.
Bivigou-Koumba gratefully acknowledges a personal grant from
Deutscher Akademischer Austauschdienst (DAAD).},
abstract = {We investigate concentrated solutions of
poly(styrene-b-N-isopropyl acrylamide) (P(S-b-NIPAM))
diblock copolymers in deuterated water (D2O). Both
structural changes and the changes of the segmental dynamics
occurring upon heating through the lower critical solution
temperature (LCST) of PNIPAM are studied using small-angle
neutron scattering and neutron spin-echo spectroscopy. The
collapse of the micellar shell and the cluster formation of
collapsed micelles at the LCST as well as an increase of the
segmental diffusion coefficient after crossing the LCST are
detected. Comparing to our recent results on a triblock
copolymer P(S-b-NIPAM-b-S) [25], we observe that the
collapse transition of P(S-b-NIPAM) is more complex and that
the PNIPAM segmental dynamics are faster than in
P(S-b-NIPAM-b-S).},
keywords = {J (WoSType)},
cin = {ICS-1 / JCNS (München) ; Jülich Centre for Neutron
Science JCNS (München) ; JCNS-FRM-II / JCNS-1},
ddc = {540},
cid = {I:(DE-Juel1)ICS-1-20110106 /
I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-1-20110106},
pnm = {BioSoft: Makromolekulare Systeme und biologische
Informationsverarbeitung / Großgeräte für die Forschung
mit Photonen, Neutronen und Ionen (PNI)},
pid = {G:(DE-Juel1)FUEK505 / G:(DE-Juel1)FUEK415},
experiment = {EXP:(DE-MLZ)J-NSE-20140101 / EXP:(DE-MLZ)KWS2-20140101},
shelfmark = {Chemistry, Physical / Polymer Science},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000289576300024},
doi = {10.1007/s00396-011-2382-3},
url = {https://juser.fz-juelich.de/record/15283},
}